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Lancaster • Laboratories Page 1 of 5 Lancaster Laboratories Sample No. WW 3996002 Collected 02/12/2003 10 10 by FT Account Number 10906 Submitted 02/14/2003 09 20 ChevronTexaco Reported 02/27/2003 at 18 52 6001 Bollinger Canyon Rd L4310 Discard 03/30/2003 MW-1-W-030212 Grab Water San Ramon CA 94583 Facility# 92033 Job# 386847 GRD 508 Charter Way 70607700702 MW-1 033M1 As Received CAT As Received Method Dilution No Analysis Name cAs Number Result Detection units Factor Limit 01728 TPH-GRO - Waters n a 77 50 ug/1 1 The reported concentration of TPH-GRO does not include MTBE or other gasoline constituents eluting prior to the C6 (n-hexane) TPH-GRO range start time A site-specific MSD sample was not submitted for the pro3ect A LCS/LCSD was performed to demonstrate precision and accuracy at a batch level 05553 TBH - DRO CA LUFT (Waters) n a 3,000 130 ug/1 5 According to the California LUFT Protocol, the quantitation for Diesel Range Organics was performed by peak area comparison of the sample pattern • to that of our #2 fuel oil reference standard (between C10 and C28 normal hydrocarbons) Site-specific MS/MSD samples were not submitted for the prosect A LCS/LCSD was performed to demonstrate precision and accuracy at a batch level 01126 TRPH 418 1 n a 1,00 } 250 ug/l 1 Sufficient sample volume was not availpble to perform a MS/MSD for this analysis Therefore, a LCS/LCSD was performed to demonstrate precision and accuracy at a batch level 04678 TCL SW846 Semivolatiles/Waters 03871 4-Chloroaniline 106-47-8 N D 25 ug/l 1 03905 2-Methylnaphthalene 91-57-6 N D 5 ug/l 1 03907 2-Nitroaniline 88-74-4 N D 10 ug/1 1 03922 2,4,5-Trichlorophenol 95-95-4 N D 10 ug/l 1 03924 2-Chlorophenol 95-57-8 N D 5 ug/1 1 03925 Phenol 108-95-2 N D 5 ug/l 1 03926 2-Nitrophenol 86-75-5 N D 10 ug/l 1 03927 2,4-Dimethylphenol 105-67-9 N D 5 ug/l 1 03928 2,4-Dichlorophenol 120-83-2 N D 5 ug/1 1 03929 4-Chloro-3-methylphenol 59-50-7 N D 5 ug/1 1 03930 2,4,6-Trichlorophenol 88-06-2 N D 10 ug/1 1 03936 bis(2-Chloroethyl)ether 111-44-4 N D 5 ug/l 1 03937 1,3-Dichlorobenzene 541-73-1 N D 5 ug/1 1 03938 1,4-Dxchlorobenzene 106-46-7 N D 10 ug/l 1 03939 1,2-Dichlorobenzene 95-50-1 N D 5 ug/1 1 03941 Hexachloroethane 67-72-1 N D 5 ug/l 1 03942 N-Nitroso-di-n-propylamine 621-64-7 N D 5 ug/1 1 03943 Nitrobenzene 98-95-3 N D 5 ug/1 1 03944 isophorone 78-59-1 N D 5 ug/1 1 . 03945 bis(2-Chloroethoxy)methane 111-91-1 N D 5 ug/1 1 03946 1,2 4-Trichlorobenzene 120-82-1 N D 5 ug/1 1 #=Laboratory MethodDetection Limit exceeded target detection limit N D=No( detected at or abo'MKXjA.Tan9'iTUeMh M E M B F_ R Po Box 12425 s Lancaster PA 17605 2425 717-656 2300 Fax 717-656-2681 2716 RPv 10171n2