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Analysis • • <br /> Lancaster Laboratories Page 2 of <br /> Where quality is a science <br /> Quality Control Summary <br /> Client Name Chevron Products Company Group Number 797430 <br /> Reported- 03/04/02 at 04 09 PM <br /> Laboratory Compliance Quality Control <br /> Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result MDL Units %REC %REC Limits RPD RPD Max <br /> Acenaphthylene N D 5 ug/l 81 85 71-116 4 30 <br /> Dimethylphthalate N D 5 ug/1 25 26 2-102 4 30 <br /> 2,6-Dinitrotoluene N D 10. ug/l 81 86 74-120 7 30 <br /> Acenaphthene N D 5 ug/l 76 BO 68-114 5 30 <br /> 2,4-Dinitrotoiuene N D 10. ug/1 82 86 75-129 4 30 <br /> Fluorene N D 5 ug/l 75 78 63-126 4 30 <br /> 4-Chlorophenyl-phenylether N D 5 ug/l 77 61 64-121 5 30 <br /> Diethylphthalate N ❑ 5 ug/l 56 59 28-120 5 30 <br /> N-Nitrosodzphenylamxne N D 5 ug/l 75 80 64-118 6 30 <br /> 4-Bromophenyl-phenylether N D 5 ug/l 77 83 70-120 8 30 <br /> Hexachlorobenzene N D 10 ug/l 80 89 65-128 10 30 <br /> Phenanthrene N D 5 ug/1 71 78 67-116 9 30 <br /> Anthracene N D 5 ug/l 73 79 66-116 8 30 <br /> Di-n-butylphthalate N D 10. ug/1 68 72 68-119 6 30 <br /> Fluoranthene N D 5 ug/l 71 75 66-118 5 30 <br /> Pyrene N D 5 ug/1 91 100 68-125 10 30 <br /> Butylbenzylphthalate N D 50 ug/1 75 62 55-142 10 30 <br /> Benzo(a)anthracene N D 5 ug/1 74 80 71-117 8 30 <br /> Chrysene N D 5 ug/l 82 90 69-121 10 30 <br /> 3,3'-Dichlorobenzxdine N D 10 ug/1 66 78 43-111 17 30 <br /> bis(2-Ethylhexyl)phthalate N D 10 ug/l 70* 75 72-127 6 30 <br /> 0Bi-n-octylphthalate N D 10 ug/l 85 92 75-127 7 30 <br /> enzo(b)fluoranthene N D 5 ug/1 78 87 69-120 11 30 <br /> enzo(k)fluoranthene N D 5 ug/l 78 85 70-122 8 30 <br /> Benzo(a)pyrene N D 5 ug/1 78 86 75-119 9 30 <br /> Indeno(1,2,3--cd)pyrene N D 10 ug/l 77 85 71-123 9 30 <br /> Dibenz(a,h)anthracene N D 10 ug/l 84 92 78-130 9 30 <br /> Benzo(g,h,i)perylene N D 5 ug/l 79 87 72-123 10 30 <br /> 2-Methylphenol N D 5 ug/l fib 78 64-102 13 30 <br /> 4-Methylphenol N D 5 ug/l 66 73 56-99 10 30 <br /> Benzyl alcohol N D 5 ug/l 74 83 56-99 11 30 <br /> Benzoic acid N D 10 ug/l 38 27 6-72 35* 30 <br /> Batch number 020520006A Sample number(s) 3775768 <br /> TPH - DRO CA LUFT (waters) N D 50 ug/l 106 100 54-120 6 20 <br /> Batch number 02052112601A Sample number(s) 3775768 <br /> TRPH 418 1 N D 32 mg/1 85 89 61-110 4 18 <br /> Batch number P020511AC Sample number(s) 3775766 <br /> Chloromethane N D 2 ug/l 93 44-118 <br /> Vinyl Chloride N D 1 ug/l 98 55--121 <br /> Bromomethane _ N D 2 ug/l 68 34-126 <br /> Chloroethane N D 2 ug/1 74 53-117 <br /> Trichlorofluoromethane N D 2 ug/l 99 54-142 <br /> 1,1-Dichloroethene N D 1 ug/l 103 67-140 <br /> Methylene Chloride N D 2 ug/l 97 84-128 <br /> trans-1,2-Dzchloroethene N D 1 ug/1 98 83-129 <br /> 1,1-Dichloroethane N D 1 ug/1 98 77-129 <br /> cis-1,2-Dichloroethene N D 1 ug/l 97 85-126 <br /> Chloroform N D 1 ug/l 95 86-124 <br /> 1,1,1-Trichloroethane N D 1 ug/l 93 83-127 <br /> *-Outside of specification <br /> The result for one or both determinations was less than five times the LOQ <br /> The background result was more than four times the spike added <br /> Lancaster Laboratories inc <br /> IVI E PA B E R 2425 New Holland Pike <br /> PO Box 12425 <br /> Lancaster PA 17605 2425 <br /> 717-656-2300 Fax 717-656 2681 2216 Rev 9/11/00 <br />