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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike PO Box 12425 Lancaster PA 17605-2425-717-656,2300 Fax 717 656-2681•www Iancasterlab9 corn <br /> Page 4 of 6 <br /> Quality Control Summary <br /> Client Name C1levronT'exaco Group Number 921483 <br /> Reported 12/07/04 at 02 32 PM <br /> Sample Matrix Quality Control <br /> MS MSD MS/MSD RPD BRC; DUP DUP Dup RPD <br /> Analysis Name %RHC RBC Limits RPD MAX Conn Conc RPD Max <br /> Batch number N043291AB Sample number(s) 4409323 <br /> Methyl Tertiary Butyl Ether 94 91 69-134 1 30 <br /> Chloromethane 116 109 69-157 6 30 <br /> Vinyl Chloride 114 111 70-151 3 30 <br /> Bromomethane 87 81 59-143 7 30 <br /> Chloroethane 98 92 63-142 6 30 <br /> Trichlorofluoromethane 122 118 67-163 3 30 <br /> 1,1-Dichloroethene 98 96 78-146 2 30 <br /> Methylene Chloride 92 91 79-133 2 30 <br /> trans-1,2-Dichloroethene 95 95 82-133 0 30 <br /> 1,1-Dichloroethane 94 93 85-135 1 30 <br /> cis-1,2-Dichloroethene 98 96 83-126 2 30 <br /> Chloroform 102 101 82-131 1 30 <br /> 1 1,1-Trichloroethane 100 98 81-142 2 30 <br /> Carbon Tetrachloride 101 100 73-144 1 30 <br /> Benzene (2) (2) 83-128 1 30 <br /> 1,2-Dichloroethane 132 128 73-136 3 30 <br /> Trichloroethene 101 98 75-135 3 30 <br /> 1,2-Dichloropropane 98 97 81-121 1 30 <br /> Bromodichloromethane 99 '1 99 80-129 0 30 <br /> Toluene 96 95 83-127 1 30 <br /> 1,1,2-Trichloroethane 108 106 77-125 2 30 <br /> Tetrachloroethene 104 103 78-133 1 30 <br /> Dibromochloromethane 95 96 73-119 0 30 <br /> Chlorobenzene 96 97 83-120 1 30 <br /> Ethylbenzene 97 92 82-129 1 30 <br /> m+p-Xylene (2) (2) 82-130 1 30 <br /> o-Xylene 102 97 82-130 2 30 <br /> Bromoform 96 95 64-119 1 30 <br /> 1,1,2,2-Tetrachloroethane 93 92 69-121 1 30 <br /> 1,3-Dichlorobenzene 101 100 79-123 0 30 <br /> 1,4-Dichlorobenzene 99 97 81-122 1 30 <br /> 1,2-Dichlorobenzene 99 98 82-117 0 30 <br /> trans-1,3-Dictiloropropene 93 92 75-117 1 30 <br /> cis-1,3-Dichloropropene 98 97 76-117 1 30 <br /> Freon 113 107 105 73-166 2 30 <br /> Batch number Z043301AA Sample number(S? 4409322,4409325-4409326 <br /> Methyl Tertiary Butyl Ether 107 100 69-134 3 30 <br /> Benzene 95 72* 83-128 14 30 <br /> Toluene 108 106 83-127 2 30 <br /> Ethylbenzene 115 114 82-129 1 30 <br /> Xylene (Total) 114 113 82-130 1 30 <br /> Surrogate Quality Control <br /> Analysis Name TCL SW846 Semivolatlles/Waters <br /> Batch number 04324WABO26 <br /> 2-Fluorophenol Phenol-d6 2,4,6-Tribromophenol Nitrobenzene-d5 <br /> 4409323 55 36 95 87 <br /> *-Outside ofspecification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br />