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OilLancasteris Re orf <br /> Laboratories A n a l ys p <br /> 2425 New Holland Pike PO Box 12425 Lancaster PA 17605 2425•717 656 2300 Fax 717-856 2681•www lancasterlabs Com <br /> Page 5 of 8 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 907633 <br /> Reported 09/01/04 at 08 32 AM <br /> Sample Matrix Quality Control <br /> MS MSD MS/MSD RPD EKG DUP DUP Dup RPD <br /> Analysis Name SLREC $REC Lim2t8 RPD MAX Conc Conc RPD Fax <br /> Di-n-octylphthalate 98 98 55-119 0 30 <br /> Benzo(b)fluoranthene 96 96 69-114 2 30 <br /> Benzo(k)fluoranthene 100 100 68-117 0 30 <br /> Benzo(a)pyrene 98 96 70-115 1 30 <br /> Indenc(1 2,3-cd)pyrene 96 97 69-118 1 30 <br /> Dibenz(a h)anthracene 108 109 73-126 1 30 <br /> Benzo(g,h,i)perylene 98 98 70-117 0 30 <br /> 2-Methylphenol 75 76 30-115 1 30 <br /> 4-Methylphenol 72 74 24-118 3 30 <br /> Benzyl alcohol 77 79 61-69 3 30 <br /> Benzoic acid 0* 18 6-60 200* 30 <br /> Batch number 042270002A Sample numbers) 4329995 <br /> TPH - DRO CA LUFT (Waters) 122 133• 59-128 10 20 <br /> Batch number 042271848002 Sample number(s) 4329996 <br /> Cadmium 104 107 87-117 2 20 N D N D 0 (1) 20 <br /> Chromium 99 101 86-118 2 20 0 0034 0 0033 2 (1) 20 <br /> Lead 101 103 87-118 2 20 N D N D 0 (1) 20 <br /> Nickel 103 105 91-111 2 20 0 0036 0 0042 16 (1) 20 <br /> Zinc 102 104 80-120 2 20 0 0054 0 0060 12 (1) 20 <br /> Batch number 04233112601A Sample number(a) 4329995 <br /> 1 1 1 0 8 (I) 34 <br /> TRPH 418 1 <br /> Batch number N042261AD Sample number(s) 4329995 <br /> Methyl Tertiary Butyl Ether 92 92 69-134 0 30 <br /> Chloromethane 108 112 69-157 4 30 <br /> Vinyl Chloride 110 114 70-151 4 30 <br /> Bromomethane 98 98 59-143 0 30 <br /> Chloroethane 104 106 63-142 2 30 <br /> Trichlorofluoromethane 115 115 67-163 0 30 <br /> 1 1-Dlchloroethene 108 110 78-146 2 30 <br /> Methylene Chloride 102 99 79-133 3 30 <br /> trans-1 2-Dichloroethene 102 102 82-133 0 30 <br /> 1 I-Dichloroethane 108 106 85-135 2 30 <br /> cis-1,2-D2chloroethene 108 104 83-126 4 30 <br /> Chloroform 113 111 62-131 2 30 <br /> 1 1,1-Trichloroethane 115 112 81-142 2 30 <br /> Carbon Tetrachloride 114 111 73-144 2 30 <br /> Benzene 113 111 83-128 2 30 <br /> 1 2-Dichloroethane 109 106 73-136 3 30 <br /> Trichloroethene 110 107 75-135 3 30 <br /> 1 2-Dschloropropane 111 109 81-121 2 30 <br /> Bromodichloromethane 109 106 80-129 3 30 <br /> Toluene 110 109 83-127 1 30 <br /> 1,1,2-Trichloroethane 105 105 77-125 0 30 <br /> Tetrachloroethene 106 104 78-133 2 30 <br /> Dxbromochloromethane 101 99 73-119 2 30 <br /> Chlorobenzene 104 103 83-120 1 30 <br /> Ethylbenzene 107 106 82-129 0 30 <br /> mop-xylene 108 107 82-130 1 30 <br /> o-Xylene 103 101 62-130 1 30 <br /> Bromoform 92 92 64-119 0 30 <br /> 1 1,2 2-Tetrachloroethane 103 103 69-121 0 30 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five Mmes the LOQ <br /> (2) The background result was more than four times the spike added <br />