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Spargero Analytical Laboratory Division <br /> Techno"yInc <br /> Mobile Laboratory Division <br /> Scientific Division <br /> With Automotion in <br /> EPA Method 8240/8260 Modified GCMS <br /> Matrix Spike (MS) and Matrix Duplicate Spike (MSD) <br /> Attention Mr Claudio Avila Date Samoled Nov 25, 1996 <br /> EMCON Date Received Nov 26, 1996 <br /> 1433 North Market Blvd Date Analvzed Dec 2, 1996 <br /> Sacramento, CA 95834 Invoice# 7238 <br /> Protect# 22613-100 001 Protect Name Don Rogers <br /> Client ID MS/MSD (Batch) LAB ID 7226-039MS <br /> 7226-039MSD <br /> Matrix Water Dilution <br /> UNITS = ug/1 <br /> Sample Spike MS MSD QC Limits <br /> Compound Conc Added MS MSD % Rec % Rec RPD RPD % Rec <br /> 1,1-Dichloroethene ND 50 64 70 128% 140% 9% 20 61-190 <br /> Benzene ND 50 76 76 152% 152% 0% 20 76-190 <br /> Trichloroethene ND 50 61 66 122% 132% 8% 20 71-190 <br /> Toluene ND 50 76 78 152% 156% 3% 20 76-190 <br /> Chlorobenzene ND 50 69 70 138% 140% 1% 20 75-190 <br /> ppb-parts per billion=ugll=micrograms per liter <br /> ppm=parts per million=ug/ml=micrograms per milliliter <br /> ND=Not Detected Compound{s)maybe present at concentrations below the detection hmil <br /> Dec 24, 1996 <br /> R L James, Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY INC IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certfication No 16's) <br /> 82GOMSW XLS <br /> 3050 Fite Circle Suite 112 - Sacramento Colifornfc =--:'-:',27 - (916) 362-6947 - FAX (946) 362-0947 <br />