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3 <br /> SEQUOIA ANALYTICAL <br /> 680 Chesapeake Drive • Redwood City, CA 94063 <br /> (415) 364-9600 * FAX (415) 364-9233 <br /> Blaine Tech Services, Inc Client Project ID Shell, 620 W Charter Way, Stockton Sampled Aug 27, 1993 <br /> 985 Timothy Drive Sample Matrix Sludge Received Aug 30, 1993 <br /> San Jose, CA 95133 Analysis Method EPA 5030/8015/8020 Reported Sep 9, 1993 <br /> Attention Jim Keller First Sample # 3HE7804 <br /> TOTAL PURGEABLE PETROLEUM HYDROCARBONS with BTEX DISTINCTION <br /> Reporting Sample <br /> Analyte Limit I D <br /> mg/kg 3HE7804 <br /> MW-5 <br /> Purgeable <br /> Hydrocarbons 1 0 N D <br /> Benzene 00050 N D <br /> Toluene 00050 N D <br /> Ethyl Benzene 00050 N D <br /> Total Xylenes 00050 N D <br /> Chromatogram Pattern <br /> Quality Control Data <br /> Report Limit <br /> Multiplication Factor 1 0 <br /> Date Analyzed 9/5/93 <br /> Instrument Identification GCHP-18 <br /> Surrogate Recovery, % 87 <br /> (OC Limits = 70-130%) <br /> Purgeable Hydrocarbons are Guantitatea against a fresh gasoline standard <br /> Analytes reported as tai 0 were not detected above the stated reporting limit <br /> / lA ANA6T�ICAL <br /> I <br /> Apbgg)& P <br /> Pfo�ir anager 3HE7801 BLA <3> <br />