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' 110 2nd Avenue South #D7,Pacheco,CA 94553-5560 <br /> 4 MCCA /2BELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell corn E-mail main@rnecampbell cont <br /> Advanced GcoEnvironmental TChent Project ID K& S Gas& Grocery Date Sampled 11/02/01 <br /> 837 Shaw Road <br /> Date Received 11/06/01 <br />' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 11/13-11/14/01 <br /> Client P O Date Analyzed 11/13-11/14/01 <br /> Volatile Organics By GC/MS <br />' EPA method 8260 <br /> Lab 1D --- - - 82832 � - - - -- <br />' Client 1D - CPT-4-147` <br /> Matrix W <br /> NReportingl,,mstCompound Gancentration* Compound Goncentrahon* w S <br /> Acetone(° NDc10 25 trans-1,3-Dichloropropene ND 1 0 50 <br /> Benzene 58 I 0 5 0 Ethylene d)bromide ND l U 5 0 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND , 0 1 50 <br />' Bromochloromethane ND 1 0 5 0 liexachlorobutadiene ND 5 D 1 25 <br /> Bromodichloromethane ND 1 0 50 lodomethane ND 1 0 5 0 <br /> Bromoform I ND 1 0 5 0 Isopropylbenzene ND 1(! 5 0 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 S C <br />' n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND l 0 c U <br /> sec-Bury'benzene ND 1 05 0 Methylene Chlorsde e1 ND 1 0 5 t <br /> tent-Butyl benzene ND 10 S 0 Methyl ethyl ketone 3 2 20 1 C' <br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone ND l 0 5 U <br /> lieCarbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Fther(MT131-,) - 10 50 <br /> 11 Chlorobenzene ND 1-0 7-50 Naphthalene ND 56 5 0 <br /> Chloroethane ND 10 50 n-Propyl benzene ND 10 50 <br /> C'hloroethyl Vinyl Ether` ND 0 5 0 Styrene ND 1 0 50 <br /> Chloroform ND 1 0 50 1 1 1 2-Tetrachloroethane ND U 5 0 <br /> Chloromethane ND ¢ 1 0 50 1 1,2,2-Tetrachloroethane ND 10 5 0 <br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 10 5 0 <br /> 4-Chlorotoluene ND 1 0 5 0 Toluene ND <br /> 10 S Q <br />' Dlbromochloromethane ND 1 0 5 0 1,2 3-Tnchlombenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnehlorobenzene ND 5 25 <br /> Dibromomethane ND 10 50 1,1,1-Tnchloroethane ND 10 <br /> 1 2-Dichlorobenzene ND rio <br /> 5 0 1 1,2-Tnchloroethane ND 10 5 0 <br />' 1,3-Dichlorobenzene ND S U Trichloroethene ND 10 5 0 <br /> 1 4-Dichlorobenzene ND 5 0 Trichlorofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 5 0 1,2,3-Tnchloropropane ND 10 5 G <br /> 1 1-Dichloroethane ND 5 0 1 2 4-Tnmethylbenzene ND l 0 5 0 <br />' 1,2-Dichloroethane ND 5 0 1,3,5-Tnmethy1bmzene ND -10 5 0 <br /> l,l-Dichloroethene ND 1 0 .50 Vinyl Acetate °' ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride ND 1 0 5 0 <br /> trans-l,2-Dichlomethene ND 1 0 50 Xylenes,total °' ND 10 5 C <br />' 1 2-Dichloropropane ND 1 U 5 0 Comments 1 <br /> 1 3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%) <br /> 2 2-Dichloropropane ND 1 0 50 Dibromofluoromethane 115 <br />' 1,1-Dichloropropenc ND 1 0 5 0 Toluene-d8 94 <br /> cis-1,3-Dtchloropropene ND 20. 1 5.0 4-Bromotluorobenzene )02 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroetboxy) ethene, (d) 2-hexanone (e) dichloromethane (0 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present, (1) liquid sample that contains greater than--5 vol °/ <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (i) methylbenzene (m) acetic acid ethenyl ester (n) <br />' chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> 1 <br />