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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' httn//www mccampbell corn E-mail main@mccampbell cam <br />' Advanced GeoEnvtronmental Client Project ID K& S Gas ! Date Sampled 09/14/01 <br /> 837 Shaw Road Date Received 09/18/01 <br />' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 09/27/01 <br />' <br /> ECIlent P O Date Analyzed 09/27/01 <br /> Seven Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 m_odrfed <br />' Lab ID 78857 78858 78859 <br /> MW1/ MW2/ MW3/ Reporting Limit <br /> Client ID 091401 091401 091401 <br />' Matrix TND<50 <br /> W I W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(D1PE) ND<25 ND<50 � 50 1 0 <br /> Ethyl tert-Butyl Ether(ETRE) 0 ND<25 ND<50 50 1 0 <br /> Methyl tert-Butyl Ether(MTBE) 320 ND<25 160 so 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND<50 ND<25 ND<50 50 1 0 <br />' ND<250 ND<12S ND<250 25 5 0 <br />' Methanol ND<25,000 ND<12,500 ND<25,000 2500 500 <br /> tert-Butanol <br /> Ethanol ND<2500 ND<1250 ND<2500 250 50 <br /> Surrogate Recoveries{%) <br /> Dibromonuoromethane 94 [:93 91 <br />' Comments <br />' *water samples are reported in ug/L soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting lima,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />