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110 2nd Avenue South,#lD7,Pacheco,CA 94553-5560 <br /> McCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> littp//www riieLAbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID K&S Gas&Grocery <br /> Date Sampled 06/20/01 <br /> Date Received 06/21/01 <br /> 837 Shaw Road j <br />' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 06/21-06/22101 <br /> Client P O Date Analyzed 06121-06122/01 <br />' Seven Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br />' Lab ID 70397 70398 70399 <br /> Reporting Lirtut <br /> Client ID MWi/062000 MW2/062000 MW3/062000 <br />' Matrix W W W S W <br /> Compound Concentration* uPg ug/L <br /> Di-isopropyl Ether(DIPE) ND<10 ND<10 ND<85 50 10 <br />' Ethyl tert-Butyl Ether(E"L"BE) ND<10 ND<10 ND<85 50 10 <br /> Methyl tert-13uty1 Ether(MTBE) 320 ND<l 0 110 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND<10 ND<10 ND<85 50 10 <br /> tert-Butanol ND<50 ND<50 ND<430 25 50 <br />' Methanol ND<5000 ND<5000 ND<43,000 1000 500 <br /> Ethanol ND<500 ND<500 ND<4300 250 50 <br /> Surrogate Recoveries{%) <br /> Dibromofluoromethane 98 100 100 <br /> ' Comments J <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br /> ' ND means not detected above the reporting lumt,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> ' high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />