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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccatnpbell com E-mail main@mccampbell cam <br /> Advanced GeoEnvironmental Client Project ID K&S Gas&Grocery Date Sampled 03/19/2001 <br /> 837 Shaw Road Date Received 03/20/2001 <br /> IStockton, CA 95215 Client Contact Calvin Lee Date Extracted 03/20/2001 <br /> Client P O Date Analyzed 03/20/2001 — <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 63393 63394 63395 <br /> Reporting Limit <br /> Client ID MWI/03-19-01 MW2/03-19-01 MW3/03-19-01 <br /> Matrix W W W S W <br /> Compound Concentration* ug/kg uglL <br /> Di-isopropyl Ether(DIPE) ND<100 ND<100 ND<100 50 10 <br /> Ethyl tent-Butyl Ether(ETRE) ND<100 ND<100 ND<100 5 0 10 <br /> • Methyl-tert Butyl Ether(MTBE) 330 ND<100 160 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND<100 ND<100 ND<100 50 10 <br /> tert-Butanol ND<500 ND<500 ND<500 25 50 <br />' Methanol ND<20,000 ND<20,000 ND<20,000 1000 200 <br />' Ethanol ND<5000 ND<5000 _ ND<5000 250 50 <br /> Surrogate Recoveries(%) <br />' Dibromofluoromethane 115 118 115 <br />' Comments <br />' *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />