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Castle Analytical Laboratory,Atwater, CA <br /> Lab Report No H3011011 Date 01/20/2003 Page 13 <br /> Protect Name DARPETRO#8 Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No NA Method 8260FA <br />' Prep Meth SW5030B <br /> Field ID MW-9 Lab Samp ID 5374-9W <br /> DescrlLocation MW-9 Recd Date 01/10/2003 <br /> Sample Date 01/09/2003 Prep Date 01/13/2003 <br /> Sample Time 1300 Analysis Date 01/13/2003 <br />' <br /> Matrix Water QC Batch VWMS-1133 <br /> Bass Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pic DEI <br />' Methyl-tert-butyl ether(MTBE) 0 289 05 MRL 2a UG1L 1 <br /> Ethyl tert-butyl ether(ETBE) 0 084 05 MRL ND UGIL 1 <br />' tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UGI!_ 1 <br /> Di-isopropyl ether(DIPE) 0155 05 MR!_ Q61 UGIL 1 <br /> tert-Butyl alcohol BA) 1 879 20 MRL 79L UGIL 1 <br />' SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 76-129 SLSA 110% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 104% 1 <br /> 1 <br /> 1 <br /> 1 <br />' <br /> Approved by � Date <br /> Pp , <br />