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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No H4072004 Date 07/30/2004 Page 3 <br /> 17 Project Name DARPETRO#8 Analysts Volatile Organic Compounds by GC/MS Fuel <br /> Project No NA Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-11 Lab Samp ID 7178-11W <br /> Descr/Location MW-11 Rec'd Date 07/20/2004 <br /> Sample Date 07/19/2004 Prep Date 07/27/2004 <br />' Sample Time 0838 Analysis Date 07/27/2004 <br /> Matnx Water QC Batch VWMS-7274 <br /> Basis Not Filtered Notes <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0 289 05 MRL R2 UGIL 1 <br /> Ethyl ter,-butyl ether(ETRE) 0 084 05 MRL ND UGIL 1 <br />' tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UGIL 1 <br /> Di-isopropyl ether(DIPS) 0155 05 MRL ND UGIL 1 <br /> tert-Butyl alcohol (TBA) 879 20 MRL 72 UGIL 1 <br />' 1,2-Dichloroethane 0 081 05 MRL 12 UGIL 1 <br /> 1,2-Drbromoethane 1 0 092 05 MRL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br />' Toluene-d8 63-132 SLSA 108% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 111% 1 <br /> 1• <br /> 1 <br /> Approved by Date <br />