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Castle Analytical Laboratory, Atwater, CA <br />' Lab Report No H4010717 Date 01/16/2004 Page 5 <br /> Protect Name DARPETRO#8 Analysis Volatile Organic Compounds by GC/MS Fuel <br />' Protect No NA Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-13 Lab Samp ID 6508-13W <br /> Descr/Location MW-13 Recd Date 01/08/2004 <br /> Sample Date 01/06/2004 Prep Date 01/12/2004 <br />' Sample Time 1150 Anaiysis Date 01/12/2004 <br /> Matnx Water QC Batch VWMS-1124 <br /> Basis Not Filtered Notes <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Dd <br /> Methyl-tert-butyl ether(MTBE) 0 289 06 MRL ND UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 0 084 05 MRL ND UG/L 1 <br />' tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPE) 0155 05 MRL ND UG/L 1 <br /> tett-Butyl alcohol BA <br /> 879 20 MRL ND UG/L 1 <br />' SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 76-129 SLSA 120% 1 <br /> 1,2-0ichloroethane-d4 53-141 SLSA 938% 1 <br /> 1 <br /> I <br /> I <br /> • <br /> Approved by- _ Date <br />