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tCastle Analytical Laboratory, Atwater, CA <br />' Lab Report No h3100901 Date 10/20/2003 r Page 6 <br /> Project Name DARPETRO#8 Analysis Volatile Organic Compounds by GC/MS Fuel <br />' Protect No NA Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-5 Lab Samp ID 6206-4W <br /> DescrlLocation MW-5 Rec'd Date 10/09/2003 <br /> Sample Date 10/08/2003 Prep Date 10/15/2003 <br />` Sample Time 1410 Analysis Date 10/15/2003 <br />' <br /> Matrix Water OC Batch VWMS-0153 <br /> Basis Not Filtered Notes BH <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Dd <br /> Methyl-tent-butyl ether(MTBE) 145 25 MRL 83 UG/L 5 <br />' Ethyl tert-butyl ether(ETBE) 0 420 25 MRL ND UGIL 5 <br /> tent-Amyl methyl ether (TAME) 0 335 25 MRL ND UGIL 5 <br /> Di-isopropyl ether(DIPS) 0 775 25 MRL ND UG/L 5 <br />' tert-Butyl alcohol (TBA) 440 100 MRL ND UGIL 5 <br /> 1,2-Dichloroethane 0 405 25 MRL ND UGIL 5 <br /> 1,2-Dibromoethane 046 25 MRL ND UG/L 5 <br />' SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 76-129 SLSA 884% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 943% 1 <br />' BH Reporting limits raised due to high level of non-target analytes <br /> I <br /> I <br /> Approved by -- _ Date U <br />