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' CASTLE ANALYTICAL LABORATORY <br /> ! Environmental Testing Services 2333 Shuttle Drive Atwater, CA 95301 Phone (209)384-2930 <br />' <br /> Certificate#2480 <br /> Fax (209)384-1507 <br /> Consolidated Testing Laboratories, Inc Client Project ID Beneto#8 Method EPA 5030I8015M,8020 <br /> 603 E Worth Ave Reference Number 8403 instrument ID Var-GC1 <br />' Porterville,CA 93257 Sample Description Water Extracted 08-01-05 <br /> Attn David Harris Analyst Jim Phillips Analyzed 08-01-05 <br /> Reported 08-10-05 <br /> QUALITY CONTROL DATA REPORT <br /> 1 <br /> ANALYTE Gasoline MTBE Benzene Toluene Ethyl Benzene Total Xylenes <br /> Spike Concentration 110 2 16 1 34 7 58 182 8 88 <br />' Units uglL ug/L ug/L ug/L ug/L uglL <br /> LCS Batch# VW-8015 VW-8015 VW-8015 VW-8015 VW-8015 VW-8015 <br />' LCS%Recovery 936% 983% 108% 104% 110% 107% <br /> Surrogate Recovery 101% 978% 978% 978% 978% 978% <br /> Control Limits 70-130% 70-130% 70-130% 70-130% 70-130% 70-130% <br /> MS/MSD Batch# VW-8015 VW-8015 VW-8015 VW-8015 VW-8015 VW-8015 <br />' Spike Concentration 110 216 134 758 182 888 <br /> MS%Recovery 894% 107% 108% 100% 105% 100% <br />' Surrogate Recovery 105% 102% 102% 102% 102% 102% <br /> MSD%Recovery 991% 81 3% 107% 101% 104% 101% <br /> Surrogate Recovery 104% 101% 101% 101% 101% 101% <br />' Relative%Difference 102% 265% 0903% 106% 0 321% 0166% <br />' Method Blank ND ND ND ND ND ND <br /> Surrogate Recovery 936% 930% 930% 930% 930% 930% <br />' The LCS(Laboratory Check Sample)is a control sample of known,interferent free matrix that is fortified with representative analytes and <br /> analyzed using the same reagents,preparation and analytical methods employed for the samples The LCS%recovery is used for validation <br /> of sample batch results Due to matrix effects,the QC limits and recoveries for MSIMSD's are advisory only and are not used to accept or <br />' reject batch results <br /> APPROVED BY APPROVED BY <br /> ' Clair J Cane James C Phillips <br /> Laboratory Manager Laboratory Director <br />