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' Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No H5041903 Date 04/27/2005 Page 1 <br /> Protect Name BENETO TANK LINES#8 Analysis Volatile Organic Compounds by GC/MS Fuel <br />' Protect No N/A Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-1 Lab Samp ID 8016-1 W <br /> Descr/Location MW-1 Recd Date 04/19/2005 <br /> Sample Date 04/18/2005 Prep Date 04/21/2005 <br /> Sample Time 1725 Analysis Date 04/21/2005 <br />' Matrix Water QC Batch VWMS-4215 <br /> Basis Not Faltered Notes DF <br />' Analyte Det Limit Rep Limit Note Result Units Pvc DFI <br /> Methyl-tert-butyl ether(MTBE) 578 10 MRL 31 Q UG/L 20 <br /> Ethyl tert-butyl ether(ETBE) 168 10 MRL ND UG/L 20 <br />' tert-Amyl methyl ether(TAME) 134 10 MRI_ ND UG/L 20 <br /> Di-isopropyl ether(DIPS) 31 10 MRL ND UG/L 20 <br /> tert-Butyl alcohol (TBA) 1758 200 MRL ND UG/L 20 <br />' 1,2-Dichloroethane 162 10 MRL ND UG/L 20 <br /> 1,2-Dibromoethane 184 10 MRL ND UG/L 20 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br />' Toluene-d8 63-132 SLSA 986% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 951% 1 <br /> DF Reporting limits elevated due to matrix interferences <br /> I <br /> I <br /> Approved by J Date <br />