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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No H5041903 Date 04/27/2005 Page 12 <br /> Protect Name BENETO TANK LINES#8 Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No NIA Method 8260FA <br /> Prep Meth SW50308 <br /> I Field ID MW-8 Lab Samp ID 8016-8W <br /> Deser/Location MW-8 Recd Date 04/19/2005 <br /> Sample Date 04/18/2005 Prep Date 04/21/2005 <br /> Sample Time 0940 Analysis Date 04/21/2005 <br /> Matrix Water QC Batch VWMS-4215 <br /> Basis Not Filtered Notes DF <br /> I Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0 578 1 MRL 45 UG/L 2 <br /> Ethyl tert-butyl ether(ETBE) 0 168 1 MRL ND UG/L 2 <br /> I tert-Amyl methyl ether(TAME) 0134 1 MRL ND UG/L 2 <br /> Di-isopropyl ether(DIPE) 031 1 MRL ND UG/L 2 <br /> tert-Butyl alcohol (TBA) 1758 40 MRL 47 UG/L 2 <br /> I 1,2-Dichloroethane 0162 1 MRL ND UG/L 2 <br /> 1,2-Dibromoethane 0184 1 MRL ND UG/L 2 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> I Toluene-d8 63-132 SLSA 104% 1 <br /> 112-Dichloroethane-d4 59-135 SLSA 948% 1 <br /> DF Reporting limits elevated due to matrix interferences <br /> I <br /> I ��L Z uS <br /> Approved by Date <br />