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ICastle Analytical Laboratory, Atwater, CA <br /> Lab Report No H5041903 Date 04/27/2005 Page 5 <br /> ProjectENETO TANK LINES#8 Analysis Volatile Organic Compounds by GC/MS Fuel <br /> A Method 8260FA <br />' Prep Meth SW5030B <br /> Field ID MW-13 Lab Samp ID 8016-13W <br />' Descr/Location MW-13 Recd Date 04/19/2005 <br /> Sample Date 04/18/2005 Prep Date 04/21/2005 <br /> Sample Time 1028 Analysis Date 04/21/2005 <br />' Matnx Water QC Batch VWMS-4215 <br /> Basis Not Filtered Notes <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether (MTBE) 0 289 05 MRL 22 UGIL 1 <br /> Ethyl tert-butyl ether(ETBE) 0 084 05 MRL ND UGIL 1 <br />' tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UGlL 1 <br /> Di-isopropyl ether(DIPS) 0155 05 MRL ND UGIL 1 <br /> tert-Butyl alcohol (TBA) 879 20 MRL 25: UGIL 1 <br />' 1,2-Dichloroethane 0 081 05 MRI_ ND UGIL 1 <br /> 1,2-Dibromoethane 1 0 092 05 MRL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br />' Toluene-d8 63-132 SLSA 101% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 107% 1 <br /> 1 <br /> 1 <br /> 1 <br />' <br /> Approved C r Date O T <br />