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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive, Atwater, CA 95301 Phone (209) 387-2930 <br /> Certificate #2079 Fax (209) 384-1507 <br /> Advanced GeoEnviron mental Inc Client Project ID Nomellini SampleD-9 <br /> of Northern California Reference Number 2162 Receive <br />' 4005 North Wilson Way Sample Description Water ExtractStockton, CA 95205 Sample Prep/Analysis Method EPA 5030!8015, 8020 AnalyzAttn Tim Cuellar Lab Numbers 2162-6W, 7W, 8W, 9W Reporte <br /> TOTAL PETROLEUM HYDROCARBONS -GASOLINE <br />' WITH BTEX DISTINCTION <br />' ANALYTE REPORTING LIMIT SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br /> MW-41 MW-11 MW 21 MW-3! <br /> 3-29 99 3-29-99 3-2999 3-29-99 <br /> (ug/L) (ug/L) (uglL) (uglL) (ug/L) <br /> MTBE 050 ND ND ND ND <br />' BENZENE 0 50 1800 5000 8900 13000 <br /> TOLUENE 050 ND 1200 140 3900 <br /> ETHYL BENZENE 050 270 720 830 1400 <br /> TOTAL XYLENES 050 67 1400 400 3800 <br />' GASOLINE RANGE <br /> HYDROCARBONS 50 7700 25000 21000 54000 <br />' Report Limit Multiplication Factor 100 200 200 500 <br /> ' Surrogate % Recovery FID 107%1 PID 100% FID 102%1 PID 99 7% FID 99 6%1 PID 97 5% FID 99 3%!PID 97 9% <br /> Instrument ID VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 <br /> ' Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit = Reporting Limit x Report Limit Multiplication Factor <br /> ANALYST _ _ i�A APPROVED BY <br /> CT J Cone � JS es C Phillips <br /> Lab Director <br />