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a B C LAB CRIES QUALITY CONTROL REPORT LABORATORIES (Precision & Accuracy) METHOD 5030/8020/8015M KLEINFELDER Date of Report 09/28/95 2585 EAST MYRTLE STREET Sample Matrix SOIL STOCKTON, CA 95206 Samples Affected 95-10620-1 - 95-10620-10, 95-10620-13 - 95-10620-15, 95-10620-17 95-10620-20 I I I I I MS I MSD I I I Precision) I I Accuracy QC I Sample I MS I MSD I Spike I Spike I ISpike I controt I MS I MSD I Control I j (Constituents ISample ID I Result I Result I Result I Level I Level (Units IR P D I Limits 1% Rec 1% Rec I Limits I (Benzene 110612-30 1 - 0 005 1 0 141 1 0 147 1 __0 148-__1.__ 0 148 lmglkg 1 4 ! 101 95 1, 991 80 - 1201 IToluene 10612-30 < 0 005 0 139 0 144 1 0 148 0 148 [mg/kq 4 101 93 1 97 80 1201 (Ethyl Benzene 110612-30 I < 0 005 1 0 148 I 0 154_ 0 148 I 0 148 Img/kg 1 4 1__ 101100 1104 1 80 1201 Ip&o-Xylenes 110612-30 1 0 005 1 0 288 1 0 297 I 0 296 1 0 296 1mg/kg 1 3 1 101 97_1100 1 80 1201 Im-X tene 10612-30 < 0 005 1 0 144 0 150 0 148 1 0 148 lmqlkg 1 4 1 101 97 1101 1 80 - 1201 ITPH (gas) JLCSU I < 1 0 1 6 558 I 7 027 1 7 144 1 7 144 Img/L 1 7 1 151_92 1 98 1 85 - 1151 ]surrogate 10620-1 1 1 94 70 - 1301 ISurrogate 110620-2 1 I I l I 1 1 I L88—! ! ISurrogate _110620-3 1 I I L I I I L 193 ISurrogate 110620-4 1 1 1_ I I l I 1100 I l ISurrogate 110620-5 1 I 1 1 I 1 1 199 —1 I ISurrogate 10620-6 1 100 I ISurrogate 110620-7 1 I I I I I _-1101 1 —I I ISurrogate 10620-8 1 97 ISurrogate 10620-9 J 1 91 I Isurrogate _110620-10 1 1 1 I I I 1 I _ _1. 95 l 1 ISurrogate 0620-13 1 I 1 I I 1 I _l 96 1 1 ISurrogate 10620-14 1 93 ISurrogate 10620-15 1 91 ISurrogate 110620-17 1 1 I 1 I I 1 91 1 1 ISurrogate 10620-18 1 92 ISurrogate 10620-19 1 92 ISurrogate 110620-20 1 I 1 I I I I I 1 89 I I 4 1 FK-)At G, C'-t F3,,1., 4 1it I[I i A 1)-3 3(-)k 3 t(3[715) i '7 ID1 1 FAX(805)327 1910