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California Department of Toxic Substances Control <br />Hazardous Materials Laboratory <br />Inorganic Section <br />Quality Assurance Summary for ICP <br />Number:HML 02057.8 <br />to 020578 <br />ElementBlank <br />HML Soil QC Sample <br />mg/kg <br />Method <br />m /L <br />Calibration Verification <br />Standard <br />mg/L <br />Duplicate Spiked Sample <br />HML No.: <br />020578 <br />Matrix: <br />SOLID <br />Spike Results mg/kg Unspiked Spike % Recovery <br />Result Added <br />A: B: RPD (mg/kg) (mg/kg) A: <br />B: <br />found known % <br />found known % <br />As -Arsenic <br />64.3 <br />49.5 <br />3.99 <br />19.4 <br />21.8 <br />25.4 <br />172 <br />17.1 <br />23.2 <br />25.4 <br />62.5 <br />79.9 <br />42.6 <br />128 <br />68.2 <br />50.6 <br />4.11 <br />19.3 <br />21.9 <br />25.7 <br />124 <br />18.0 <br />24.0 <br />27.1 <br />67.0 <br />88.4 <br />38.6 <br />141 <br />94.3 <br />97.8 1 <br />97.1 <br />100 <br />99.5 <br />98.8 <br />139 <br />95.0 1 <br />96.7 <br />93.7 <br />93.3 <br />90.4 <br />110 <br />90.8 <br /><0.10 <br /><0.010 <br /><0.005 <br /><0.010 <br /><0.05 <br /><0.08 <br />0.13 <br /><0.10 <br /><0.05 <br /><0.10 <br /><0.15 <br /><0.15 <br /><0.06 <br /><0.10 <br />10.6 <br />10.4 <br />10.5 <br />11.3 <br />11.0 <br />10.8 <br />9.84 <br />10.7 <br />11.2 <br />11.0 <br />10.9 <br />10.9 <br />10.3 <br />11.2 <br />10.0 <br />10.0 <br />10.0 <br />10.0 <br />10.0 <br />10.0 <br />10.0 <br />10.0 <br />10.0 <br />10.0 <br />10.0 <br />10.0 <br />10.0 <br />10.0 <br />106 <br />104 <br />105 <br />113 <br />110 <br />108 <br />98.4 <br />107 <br />112 <br />110 <br />109 <br />109 <br />103 <br />112 <br />473 <br />477 <br />99.2 <br />492 <br />485 <br />484 <br />498 <br />474 <br />487 <br />481 <br />478 <br />486 <br />465 <br />490 <br />489 <br />497 <br />103 <br />514 <br />506 <br />505 <br />521 <br />496 <br />508 <br />500 <br />496 <br />505 <br />483 <br />513 <br />3.33 <br />4.23 <br />3.76 <br />4.97 <br />4.04 <br />4.33 <br />4.80 <br />4.54 <br />4.25 <br />3.92 <br />3.70 <br />3.83 <br />3.80 <br />4.77 <br /><5.00 <br />14.3 <br /><0.25 <br />11.4 <br /><2.50 <br />9.93 <br />30.7 <br /><5.00 <br />3.12 <br />5.60 <br /><7.50 <br /><7.50 <br /><3.00 <br />18.8 <br />500 <br />500 <br />100 <br />500 <br />500 <br />500 <br />500 <br />500 <br />500 <br />500 <br />500 <br />500 <br />500 <br />500 <br />94.6 <br />92.5 <br />99.2 <br />96.1 <br />97.0 <br />94.8 <br />93.5 <br />94.8 <br />96.8 <br />95.1 <br />95.6 <br />97.2 <br />93.0 <br />94.2 <br />97.8 <br />96.5 <br />103 <br />101 <br />101 <br />99.0 <br />98.1 <br />99.2 <br />101 <br />98.9 <br />99.2.: <br />101 <br />96.6 <br />98.8 <br />Ba -Barium <br />Be -Beryllium <br />Cd -Cadmium <br />Co -Cobalt <br />Cr -Chromium <br />Cu -Copper <br />Mo -Molybdenum <br />Ni -Nickel <br />Pb -Lead <br />Se -Selenium <br />TI -Thallium <br />V -Vanadium <br />Zn -Zinc <br />Element <br />HML Liquid QC Sample <br />mg/kg <br />Reagent <br />Blank <br />mg/L__ <br />Inorganic Ventures <br />Reference Standard <br />mg/L <br />Duplicate Spiked <br />Sample <br />HML No.: <br />020593 <br />Matrix: LIQUID <br />Spike Results mg/kg Unspiked Spike % Recovery <br />Result Added <br />A: B: RPD (mg/kg) (mg/kg) A: B: <br />found known % <br />found known % <br />As -Arsenic <br />Ba -Barium <br />Be -Beryllium <br />2.59 <br />10.0 <br />2.88 <br />3.13 <br />2.66 <br />15.4 <br />65.8 <br />6.59 <br />11.7 <br />6.57 <br />14.4 <br />35.1 <br />2.35 <br />24.9 <br />2.63 <br />9.92 <br />2.97 <br />3.10 <br />2.66 <br />15.0 <br />66.1 <br />6.36 <br />11.7 <br />6.18 <br />14.1 <br />34.5 <br />2.33 <br />24.4 <br />98.5 <br />101 <br />97.0 <br />101 <br />100 <br />103 <br />99.5 <br />104 <br />100 <br />106 <br />102 <br />102 <br />101 <br />102 <br /><0.10 <br /><0.010 <br /><0.005 <br /><0.010 <br /><0.05 <br /><0.08 <br /><0.10 <br /><0.10 <br /><0.05 <br /><0.10 <br /><0.15 <br /><0.15 <br /><0.06 <br /><0.10 <br />1 1.07 <br />1.02 <br />1.03 <br />1.11 <br />1.10 <br />1.07 <br />1.08 <br />1.07 <br />1.11 <br />1.09 <br />1.08 <br />1.07 <br />1.02 <br />1.11 <br />1.00 <br />1.00 <br />1.00 <br />1.00 <br />1.00 <br />1.00 <br />1.00 <br />1.00 <br />1.00 <br />1.00 <br />1.00' <br />1.00 <br />1.00 <br />1.00 <br />107 <br />102 <br />103 <br />111 <br />110 <br />10726.0 <br />108 <br />107 <br />111 <br />109 <br />108 <br />107 <br />102 <br />111 <br />24.7 <br />24.9 <br />5.27 <br />26.2 <br />26.4 <br />34.5 <br />26.3 <br />28.2 <br />26.7 <br />26.4 <br />25.8 <br />24.8 <br />31.1 <br />25.1 <br />24.8 <br />5.22 <br />26.3 <br />26.4 <br />26.0 <br />33.8 <br />26.4 <br />28.2 <br />26.9 <br />26.3 <br />26.4 <br />24.8 <br />31.1 <br />1.21 <br />0.40 <br />0.96 <br />0.00 <br />0.00 <br />0.00 <br />2.85 <br />0.00 <br />0.00 <br />0.98 <br />0.95 <br />2.87 <br />0.00 <br />0.00 <br /><0.50 <br />0.09 <br /><0.02 <br /><0.05 <br /><0.25 <br /><0.40 <br />9.55 <br />0.60 <br />1.90 <br />1.23 <br /><0.75 <br /><0.75 <br /><0.30 <br />5.55 <br />25.0 <br />25.0 <br />5.00 <br />25.0 <br />25.0 <br />25.0 <br />25.0 <br />25.0 <br />25.0 <br />25.0 <br />25.0 <br />25.0 <br />25.0 <br />25.0 <br />98.8 <br />99.2 <br />105 <br />105 <br />106 <br />104 <br />99.8 <br />103 <br />105 <br />102 <br />106 <br />103 <br />99.2 <br />102 <br />100 <br />98.8 <br />104 <br />105 <br />106 <br />104 <br />97.0 <br />103 <br />105 <br />103 <br />105 <br />106 <br />99.2 <br />102 <br />Cd -Cadmium <br />Co -Cobalt <br />Cr -Chromium <br />Cu -Cooper <br />Mo -Molybdenum <br />Ni -Nickel <br />Pb -Lead <br />Se -Selenium <br />TI -Thallium <br />V -Vanadium <br />Zn -Zinc <br />ICP Analyst's Signature: -- (74 j ) Gurmail Sivia, PH Chemist III, Specialist: ' Gv. �' Date: l% <br />Y g `'ems <br />Chemist: U Chemist's Signature: <br />Date Analyzed: 01/03/03 -._.._n,: "`"'� <br />7 <br />