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Report Number : 36065 <br /> HFF Date : 12/29/2003 <br /> ANALYTICAL LLC <br /> Subject : 9 Soil Samples <br /> Project Name : USA PET 2448 W. KETTLEMAN <br /> Project Number: D003-004-1 <br /> Case Narrative <br /> Matrix Spike/Matrix Spike Duplicate Results associated with sample 3 B5-45, B2-15, B4-30, B1-45, B2-30, <br /> B4-45, B5-30, B1-35 and B1-30 for the analyte Methyl-t-butyl ether Were affected by the analyte <br /> concentrations already present in the un-spiked sample. TPH as Diesel was analyzed outside of hold <br /> time for samples B1-30, B1-35, and B1-45. These results are flaggE d with an 'E' and should be <br /> considered estimates. Hydrocarbons reported as TPM as Diesel do iot exhibit a typical Diesel <br /> chromatographic pattern for samples B1-30, B1-35 and B1-45. <br /> Approved By: JA� I t <br /> a � j <br /> 2795 2nd St, Suite 300 Davis, CA 95616 530-297-48001 <br />