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;_.arir1'Tem u: I GiCi- .FILStas` ti L +r� ti; _ Hazardous Materrals Laboratory HML PIUMber: AN00037 Inorganic -section to AIV00037 C Quality Assurance Summary for JCP rD MMI Soil GC Sample Method Calibration Verification Duplicate Spiked Sample NML Elio ANQ60o9 fvlatrix: SOLID C� Element Blank Standard N m9�9 rng/L Spike ResuJts mglkg Unspiked SPike % Recovery t:m found known %b found known °� A; B: Result Added 0w m . RPD imglkg) (mglkgl A: B: .. As-Arsenic 60.4 68.2 68,6 <0.05 9,57 10.0 95.7 946 952 0.63 <5.00 1000 94.6 95.2 Ba-Sarium 46,3 50.6 95.5 <0.005 9.55 10,0 95.5 548 555 1.27 1.60 1000 54.6 55.3 11�i Be Ber Ilium 3.96 4_?i 96.4 <0.003 1.96 2.00 98.0 203 203 0.00 <0.3D 2170 102 102E 3 Cd-Cadmium 1B.6 19.3 96,4 <0.005 10.5 10.fl 705 1029 1033 0,00 il 0.50 7000 103 Co-Cobalt 21.6 21.9 96.6 <0.02 10,2 ]D.0 102 1015 i 020 0,10 6.4 T OQD 98.9 700Cr-Chromium 25.6 25.799.6 <0.03 10.2 10.0 102 `•f• `*•+ Q,Op ##+ ]ODOCrr Co r 711 69.a <0.05 8.88 i0.0 86.6fuTo Mol bdenum i7.3 943 942 0.1 1 8.4 100D 92,5 92.4 �r i 18.0 86.1 <0.05 70.1 7D.0 701 997 994 0.71 8.86 1000 97.8 98.5 3D illi Mickel 24.0 24,0 100 <0.03 10.4 10.0 104 1034 1039 0.98 12.8 1000 102 103 3d Pb Lead 26.1 27.1 96.3 <0.06 10.3 10.0 103 955 963 0.63 <6A0 1000 95,5 96.3 rM o-S�'eniurn 53.6 67.0 80 <0.03 9.87 10.0 98.7 1098 3 098 0�0 9.71' 1000 709 109 `n TI-Thalhurn 76.7 88.4 86.8 <0.10 10.6 10,0 105 1088 1713 1.94 71,6 ?ODO 102 104 V-Vanadium 38,6 3$.6 100 <0.03 9.34 70.O 93.4 623 628 0.80 <2,50 1000 62.11 62.6 3 Zn-Zinc 139 141 9816 <0.04 IG-2 10.0 102 1043 1049 0.97 11.1 1000 103 i 04 TiML Liquid QC Sample Reagent Inorganic Ventures Duplicate Spiked Sample HML No,: ANOOD85 Matrix: Element Bfank Reference Standard LIQUID rng/kg mg/L Shrike Results mg/kg Unspiked Spike % Recovery found known % found known % Result Added m IL A: B: RPD Irng/kW frng/kg) A: B: As-Arsenic 2.42 2.63 92.0 <0.05 1.04 1.00 104 439 451 2.70 <2.50 500 87.13 90.2 Ba-eafium 9.50 9.92 955,8 <0.005 1.00 1.00 100 448 13 457 1,77 0.84 500 89.8 97,2 e 13e Unum 2.82 2,97 94.9 <O.OD3 0.20 0.20 100 95.3 96.4 1.15 <0.15 100 95.3 96A in Cd-Cadmium 3.13 3.10 101 <0.005 1.07 1,00 107 490 505 3.02 <0.25 500 98.0 101 Co-Cobaft o 2.64 2.68 99.2 <0.02 1.04 7.130 104 463 _Z94 2.26 1.43 500 96.3 98.5 Cr-Ghromiurn 1 fi.4 15.0 109 � <0.03 1.04 1.00 104 4136 49fi 2.04 <1.50 300 97,2 99,2 En Cu-Copper 60.9 66.1 92.1 <0.05 0-98 1 1,00 98.0 446 455 2,03 7.98 500 67.6 89_4 1 o-Mo[ bdenrrm 8.27 fi,3g 98.6 <0,05 1.09 T.00 109 47T 461 2.10 <2.50 500 84,2 g6.2 fdFNickel 11.8 71,7 10 2 <D.03 1.04 1.00 104 493 504 1.92 2.28 500 98.1 100 � €'h lead 6.47 6.18 105 <0.06 1.06 1,00 106 462 496 2.89 5.22 500 95.4 98-2o Se-Selenium 13.9 14.1 98.6 <0,08 1.02 1.00 102 470 � TI7haJlium 480 2.i 1 <4.00 500 94.0 96.0 35.2 34.5 102 <0.10 1.06 1.00 106 48B 507 3.42 <5.00 500 97.6 701 V-Vanadium 2.15 2.33 92.3 <0.03 0,97 1.00 97.0 450 455 1.70 <1.25 b00 90.0 Zn Zinc 24.1 24.4 1313.8 <0.04 1,06 o 91.0 106 566 586 3.87 86.5 500 96.3 98.9 - P Analyst's Signature: _ Lv� Chemist: Jamail Garcha, Supervisor_ Dam. �r/fid Zenaida Odi4n hernisrs Signature: =� Date Analyzed: 08/11/03 Results beyond instrument calibration. ; = Low recoveriu due to matrix interference. N