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MINIMUM VERIFICATION LABORATORY ANALYSIS <br /> OXYGEN <br /> TANK TANK TPH-G TPH-D 13TX & F CL HC TOTAL MT13F ATES NI rAt. PCB <br /> u CONTENTS SOl S 8015 8020 8010 LEAD 8020 (MTBE. ICAPI 8270 <br /> 8260 8260 8260 8240 7420 8260 TBA,DIPF., AFS or 8080 <br /> 8260 7421 FTSE. AA <br /> TAMF) <br /> X26(1 <br /> LEADED GAS X X X X <br /> UNL GAS X X X <br /> DIESEL X X <br /> KEROSENE X X X <br /> UNK FUEL X X X X X <br /> PROD.OIL X X X <br /> CHLOR. X <br /> SOLVENTS X X <br /> NONCHLOR X <br /> SOLVENTS X X <br /> WASTE`, <br /> USED OIL X X X X X X X <br /> All analysis methods are the designated EPA methods described in EPA SW 846,Third Edition. Those methods not fotmd in SW W are <br /> specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appendix D (B),Table 3-5 on page A20 for minimum detection <br /> limits for motor vehicle fuel (gasoline and diesel). Refer to "Tn-Regional Board Staff Recommendations for Initial Evaluation and <br /> Investigation of UST's" for the waste and motor oil minimum detection limits. Detection Limits that remain below the MCL,STLC or <br /> Allowable Limit of the contaminant in question will be accepted,however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-Ci Tota] Petroleum Hydrex:arbxn,Ciauiline,GCiFID 0030)901 4;mcxl ur GUMS X260 <br /> TPH-D Total Petroleum Hydrocarbon,Diesel,GC/FID(3550),X01 S mod or GC/MS 9260 <br /> BTX&F.Henzene,'I olucnc,Xylene&Fthyl Benzene,GC/PID 8020 or GC'MS 8260 <br /> CL HC Chlorinated Hydroe:arb on,CiC/IISD X010,CrC/MS X240 or X260 <br /> TOTAL LEAD 7 otal lead,AA 7420, AA 7421 or ICP-AES 6010 <br /> OXYGFNATES M"1-BF:, [-FBE,'LAME,DIPS,&"IBA GC/MS 8260(For MTHF screen only you may use 8020) <br /> METALS[CAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. Metals: <br /> Cadmiana,Chrominin III and V1,Lead,Zinc and Nickel. <br /> PCH Polychlorinated Biphenyls,GC/MS X270 or 9090 <br /> CiC-FID Gas Chromatography,Flame lonvation Detection <br /> Method 300 Acid digestion <br /> Method 3-W Soxhlet sample preparation <br /> Method 3150 Sonication sample preparation,extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: 'Io avoid false positive detection of benzene,benzene-free solvents arc to be used. Fused capillary columns are preferred to packed columns:a <br /> packed column may he used as a"first cut"with"dirty"samples or once the hydrocarbons have been charactenftd and proper QA/QC is followed For <br /> drinking water sources,FPA recommends that the S00 series for volatile organic should be used in preference to the 600 renes because the detection <br /> limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal contamination may require further analysis. PHS-EHD <br /> recommends holding those samples until disposal is indicated. <br /> FH 23 046 (Revised 05/09/00) <br /> 5 <br />