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i <br /> 0254 North Star will have tanker on site around 0800 to pump out acid tank. All acid puddle on <br /> ground neutralized with sodium carbonate. <br /> 3/5/2019 <br /> Ultrasonic test was performed at and around the leak point in the acid tank. The result of the test <br /> indicated that the metal surrounding the area is ''/a"thick and ok to weld. <br /> 4/2/2019 <br /> Tank capacity= 1500 gallons <br /> Tank was topped of 2 days' prior <br /> 1" of usage (using tape measure) from bottom plastic see through tube to the bottom of torpedo = <br /> 19.36 gals (20 gals est.) <br /> Pumped sulfuric acid from bulk sulfuric tank into 250ga1 poly totes. Total of 6 totes estimated at <br /> 230 gallons per tote for total of 1,380 gals <br /> Torpedo measurement from 0200-0830=2" or 40 gal lost <br /> Leak rate calculation(40 gal_ 390 min= 0.10256 gal/min loss or 6.15 gal/hr.) <br /> Total time of known leak 2300-1000 (11 Ins) <br /> 6.15gals * l lhrs. = 67.65gal estimated of sulfuric acid <br /> Recovered from one 55gal poly drum(3/4 filled) with remaining balance pumped from spill <br /> containment to top off one 55gal drum. Drum is processed to be ship to authorized handler <br /> Reclaimed 5gal poly drum and add back into acid tank <br /> Unable to capture through the use of poly drum, spill containment or other method due to wind <br /> as loss to the ground= 7.65 gal <br /> Total estimated time of leak prior to discovery 2100-2300 (2hrs) <br /> 6.15gal * 2hrs = 12.3ga1 estimated loss onto ground <br /> For calculation 1 gallon of 93% sulfuric acid= 15.303 lbs. <br /> Total gallons spilled or released for entire event; 67.65 + 12.3 = 79.95 gal or 1223.471bs <br /> Total captured: 55gal in poly drum+ 5gal reclaim= 60gal or 918.18lbs <br /> Total uncaptured but contained: 19.95gal or 305.291bs <br />