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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANA-LYTZCAL INC. Telephone:925-798-1620 Fax :925-798-1622 <br /> http:l/www.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project TD: Hess Dubois Cleaners Date Sampled: 10129101 <br /> 837 Shaw Road Date Received: 10/31/01 <br /> ' Stockton, CA 95215 Client Contact: Bill Little Date Extracted: 11/03-11/05/01 <br /> LirntP.O: Date Analyzed: 11/03-11/05/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 82311 <br /> Client ID MW2/102901 <br /> Matrix W <br /> Compound Concentration* Re. o ng Limit Compound Concentration' Reporting Limit <br /> W S W S <br /> ' Acetone(b) 14 5.0 25 trans-l,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> t Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 Iodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br /> ' n-Butyl benzene ND 1.0 5.0 Methyi butyl ketone ) ND 1.0 5.0 <br /> sec-Butyl benzene 2.2 1.0 5.0 Methylene Chloride"' ND[2.0 1.0 5.0 <br /> tert-Butyl benzene 1.1 1.0 5.0 Methyl ethyl ketone ' ND 2.0 10 <br /> Carbon Disulfide 9.5 1.0 5.0 Methyl isobutyl ketone o ND 1.0 5.0 <br /> Carbon Tetrachloride ND LO 5.0 Methyl tert-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlorobenzene ND 1-0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Eth ND 1.0 5.0 Styrene ND 1.0 5.0 <br /> Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachioroethene ND<2.0 1.0 5.0 <br /> ' 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br /> Dibromochloromethane ND 1.0 5.0 i,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> ' 1,2-Dichlorobenzene 1.2 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dicblorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br /> 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trirnethylbenzme ND 1.0 5.0 <br /> ' 1,2-Dichloroethane ND LO 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> IJ-Dichloroethene ND 1.0 5.0 Vinyl Acetate m ND 5.0 25 <br /> cis-1.2-Dichloroethene ND 1.0 5.0 Vinyl Chloride " ND 1.0 5.0 <br /> ' trans-l,2-Dichlormthcne ND 1.0 5.0 Xylenes,total ND 1.0 5.0 <br /> 1,2-Dicblotopropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%} <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluoromethane 89 <br /> ' 1,]-Dichloropropene ND 1.0 5.0 Toluene-dg 113 <br /> cis-1,3-Dichloropropene ND 1.0 5.0 4-Bromofluorobenzene 99 <br /> "water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug1L <br /> ' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than -5 vol.% <br /> sediment; 6) sample diluted due to high organic content; (k) ethenylbenzene; p) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> ' chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />