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110 2nd Avenue South,#D7,Pacheco,CA 94553-5 56 0 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> hM2://www.mccamnbell.com E-mail: main@mccarnpbell.com <br /> Advanced GeoEnvironmentai Client Project ID: Hess Du Bois Date Sampled:04/18-04/19/01 <br /> 837 Shaw Road Date Received:04/23/01 <br /> ' Stockton, CA 9521.5 Client Contact:Bill Little Date Extracted: 04/23/01 <br /> Client P.O: Date Analyzed:04/23-04/26/01 <br /> ' Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 65989 <br /> ' CIient ID MWIO-35 <br /> Matrix S <br /> Reporting Limit Repcxting Limit <br /> Compound Concentration* W S Compound Concentration* W S I <br /> ' Acetone(b) ND 5.0 25 bans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 Iodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND $1.05.0n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND sec-Butyl benzene ND 1.0 5.0 Methylene Chloride° ND cert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketones ND Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) --Chlorobenzene ND 1.0 5.0 Naphthalene ND <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ether"' ND 1.0 5.0 Styrene ND 1.0 5.0 <br /> ' Chloroform ND I.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene 15 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br /> ' Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibmmo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethanc ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 12,3-Tricbloropropane ND 1.0 5.0 <br /> l,l-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> ' <br /> 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acctatc m ND 5.0 25 <br /> cis-1,2-Dichloroethene 14 1.0 5.0 Vinyl Chloride " ND 1.0 5.0 <br /> trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 5.0 <br />- ' 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofiuoromethane 113 <br /> 1,1-Dichicimpropene ND 1.0 5.0 Toluene-d8 101 <br /> cis-1,3-Dichloropropene ND 1.0 5.0 1 4-13romotluorobenzene 114 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> ' (b) 2-pmpanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (i) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than-5 vol.% <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> 1 <br />