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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:9257798-1620 Fax:925-798-1622 <br /> http://www.mccaMpbell.com E-mail:main@mccampbell.com <br /> ' Advanced GeoEnvironmental Client Project ID:Hess Du Bois Date Sampled: 04/18-04/19/01 <br /> 837 Shaw Road Date Received: 04/23/01 <br /> ' Stockton, CA 95215 Client Contact:Bill Little Date Extracted: 04/23/01 <br /> [Client P.O: Date Analyzed: 04/23-04/26101 <br /> 1Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab 1D 65991 <br /> ' Client ID MW 10-45 <br /> Matrix S <br /> * Reporting Limit RkpMmg Limit <br /> Compound Concentration Compound :A Concentration* <br /> ' W 5 W 5 <br /> Acetone(°) ND 5.0 25 trans-l,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> ' Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 Iodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br /> ' n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride`O ND 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketone ND 1.0 5.0 <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) - Lo 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ether` ND 1.0 5.0 Styrene ND 1.0 5.0 <br /> ' Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tctrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoiuene ND 1.0 5.0 Tetrachloroethene 34 1.0 5,0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluenes - ND 1.0 5.0 <br /> ' Dibromochloromethanc ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 SA 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> ' 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene 10 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br /> 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> ' 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate '° ND 5.0 25 j <br /> cis-1,2-Dichloroethene 26 1.0 SAr <br /> hloride " ND 1.0 5.0 <br /> trans-l,2-Dichloroethene ND 1.0 5.0 ,total ND 1.0 5.0 <br /> ' 1,2-Dichloroprvpane ND l.0 5Ants: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0ofluoromethane 113 <br /> ' 1,1 Diehloropmpene ND 1.0 5.0 -M 100 <br /> cis-1,3-Dichloropropene ND 1.0 5.0 1 4-Bromofluorobcnzene L 116 <br /> 'water and vapor samples are reported in ug/L,sail and sludge samples in ug/kg,wipes in ug/wipe and ail TCLP/SPLP extracts in ug(L <br /> ' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b)2-propanone or dimethyl ketone; (c) (2-chlomethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (t) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than.--5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester;" (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> 1 <br />