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110 2nd Avenue South,4D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> hqp://www.mgg4MRbel1.cam E-mail:main@mccampbell.com <br /> t Client Project 1D: Hess Duboise Date-Sampled: 04/12/01 <br /> Advanced GeoEnvlronrnental � <br /> 837 Shaw Road Date Received: 04/17/01 <br /> Stockton,CA 95215 Client Contact: Bill Little Date Extracted: 04/17-04/18/01 <br /> Client P.O: Date Analyzed: 04/17-04/18/01 <br /> Volatile Halocarbons <br /> EPA method 601 or 8010 <br /> ' Lab ID 65635 65636 65637 <br /> Client ID 041201 MW5 041201 MW6 041201 MW7 <br /> Matrix W W W <br /> Com ound Concentration <br /> ' Bromodichloromethane ND ND<15 ND<5.0 <br /> Bromoform"I ND ND<15 ND<5.0 <br /> Bromomethane ND ND<15 ND<5.0 <br /> ' Carbon Tetrachloride(`) ND ND<15 ND<5.0 <br /> Chlorobenzene ND ND<15 ND<5.0 <br /> Chloroethane ND ND<15 ND<5.0 <br /> 2-Chloroethyl Vinyl Ether�d) ND ND<15 ND<5.0 <br /> Chloroform t`s 0.91 ND<15 ND<5.0 <br /> Chloromethane ND 71 ND<5.0 <br /> Dibromochloromethane ND ND<15 ND<5.0 <br /> 1,2-Dichlorobenzene ND ND<15 ND<5.0 <br /> N 1,3-Dichlorobenzene ND ND<15 ND<5.0 <br /> 1,4-Dichlorobenzene ND ND<15 ND<5.0 <br /> Dichlorodifluoromethane ND ND<15 ND<5.0 <br /> ' 1,1-Dichloroethane ND ND<15 ND<5.0 <br /> 1,2-Dichloroethane ND ND<15 ND<5.0 <br /> 1,1-Dichloroethene ND ND<15 ND<5.0 <br /> cis 1,2-Dichloroethene 1.8 830 ND<5:0 <br /> trans 1,2-Dichloroethene ND ND<15 ND<5.0 <br /> 1,2-Dichloropropane ND ND<15 ND<5.0 <br /> cis 1,3-Dichloropropene ND ND<15 ND<5.0 <br /> trans 1,3-Dichloropropene ND ND<15 ND<5.0 <br /> ' Methylene Chloride(f) ND<1.0 ND<30 ND<10 <br /> 1,12,2-Tetrachloroethane ND ND<15 ND<5.0 <br /> Tetrachloroethene 3,5 650 180 <br /> 1 1,1,1-Trichloroethane ND ND<15 ND<5.0 <br /> 1,1,2-Trichloroethane ND ND<15 ND<5.0 <br /> Trichloroethene 1.9 430 11 <br /> Trichlorofluoromethane ND ND<15 ND<5.0 <br /> ' Vinyl Chloride") ND 93 ND<5.0 <br /> %Recovery Surrogate 98 98 97 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil and sludge samples in ug/kg, wipe samples in ug/wipe <br /> Reporting limit unless otherwise stated:water/I'CLP/SPLP extracts,ND<0.5ug/L;soils and sludges,ND<5uglkg;wipes,ND<0.2ug/wipe <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> ' (b)tribromomethane;(c)tetrachloromethane;(d)(2-chloroethoxy)ethene;(e)trichloromethane;(f)dichloromethane;(g)chloroethene;(h)a <br /> lighter than water immiscible sheen is present;(i)liquid sample that contains greater than--5 vol.%sediment;0)sample diluted due to high <br /> organic content. 1 <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />