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01/10/2001 17:25 2694671118 AGE STOCKTON PAGE 04 <br /> Sent BY: McCampbell Analytical, Inc. ; 1 925 788 4612; Jan-4-01 3:46PM; Page 4111 <br /> 110 2n.d Avenue South.#D7,Pacheco,CA 94553-5560 <br /> 4 1,&CAMPBELL ANALYTICAL INC. Telephone-925-798.1620 Fax :925-798-1622 <br /> het -:/p /www,rnc nmybell,cum C.mail; main@mccampkii,com <br /> Advanced GeoEnviromnental Client Project ID: Mess Dubois Date Sample& 12/22/00 <br /> 4005 North.Wilson Way Date Received: 12/27/04 <br /> Stockton,CA 95205 Client Contact:William]little Date Extracted: 12/27-01/03101 <br /> Client P,O: .Date Analyzed: 12/27.01/03'01 <br /> Volatile Organics By GF/-MS <br /> EPA mcthud 8260 <br /> Lab 1556947 <br /> Client ID "W-1/12-2..-00 <br /> Matrix W <br /> Compound CanoentYation` RW°g is ni Compound Concentration* s`�'�440 <br /> W S <br /> Acetone N11 5.0 25 trims-l,3-Dichloropropenc NI} l.0 5.0 <br /> 13erizenc Nf) 5.0 Ethylene dibrarnide ND l.0 5.0 <br /> l3rarno onzene ND 1.0 1,0 F.thy benzene ND 1.0 s o <br /> BromuehlorurmMane Nt) 1.0 5.0 1;iexuchlorohutsdiene ND 5.0 25 <br /> 13rvmodich oromcthane ND 1.0 5A iudomethant NO (.V 5.(I <br /> Bromoeor=rt NA 1.0 5.0 Jsopropylbenzcne P I,U 5. <br /> Drornumethnne ND 1.0 5-0 p-[Aoprupyl tolueric ND 1.0 5-0 <br /> n-Butyl benzene ND I.0 5.0 lvtethyl butyl kemno' ND 1.0 5.0 <br /> scc-Auty1 berlune ND 5.0 �lethylenc Lhloridn' ND�5.0 1.0 �. <br /> terl-EJutyl berecmc FI-05-0 <br /> Methyl ethyl ketone ND 2.0 10 <br /> • Carbon Digu 1de NCI Mcthy rsr3 Utyl ketotic' ' NU 1.0 5.0 <br /> Carlson Tetra,�;,hJorido Np Methyl tern autyl thcr(M !) 1.0 5.0 <br /> Chlorobenzcne ND Naphthalene Nl'] 5.0 5.0 <br /> ('ltloroet ere NUJ n-Propyl benZerte ND l.02-chloroethyl myEtherND Sryrcne , 1} 1.0 5.9 <br /> 1,1,1,2-Tetrachloroethane Nn 1.0 5,4 <br /> C loromethane ND 1. 5.0 1,1,2,2-Tctrachlomelhane NI) 1.0 so <br /> 2-Chlonricrlucnc <br /> NO 1.0 S.0 T'ctrachleracthcne ND-5.0 i.0 5-0 <br /> 4-('hlorotoluene NU 1.0 5.0 'Toluene ND I.0 5.0 <br /> DibromochloTorneLhane ND 1.0 5. 1,2,3-TTichlorobenx rt: ND SA 25 <br /> l,2-Uibtcl=-3-chlovopropane ND 2.0 10 1.2,4Tric loroben.ene V 5.0 21 <br /> Dr rvrnornathanc No l.0 .( 1,1,1-Trichloroethonc ND _ 1.0 5.0 <br /> 1,24Vichloi-obenzenc ND 1.0 5.0 t,t,2- ch ottrettmnc ND I- 5.0 <br /> %3•Dichlombcnzene ND 1.0 5.0 Trrc areethenr: Nb 1.0 5A <br /> 1.41, c ]orobcrizene ND 10 Trchlorolluonomcihane NU 1.0 5.0 <br /> Dichlorodilluorrmethanc ND 1.0 5,0 1,2,3=frichlpropropane '1U 7.0 5.0 <br /> ,1-Dichloroethane NJ) 1755.0 1,2,4.Trimethyibenz0ne ND 1,4 5,0 <br /> ),2-Dicblmellhane ND 1.0 5. 1,7,5-Trimethylbenzenc ND I, <br /> 1,1-Dichluruet ene ND 1.0 5.0 vinyl Acetate ND 2S <br /> cit-1,2-Dichloroelhene ND 1.0 5.0 vinyl Chloride`"' ND 1.0 5.0 <br /> flans-1, - icbloract ene To 5.0 y encr,totaY ND <br /> 1,2-Dxhloropr0p2ue ND 1.0 5.0 Comments! <br /> 1,3-Dichlare mpane TWD 1.0 5.0 Surrogate Reeoverle! <br /> 2,2-UtchlurrrproDanc ND 1.0 5.0 Dibromofluororrrethane t09 <br /> 1,;-Dit:h10r0p1opcne ND 1.6-.-5.0 To3uanc-d8 101 <br /> cis. , -Dlah oropropcnc ND i A 1 5.0 4- romolluoro comma 92 <br /> 'water and vapor samples arc rcpo Md In uglL,soil and sludge samples in ug/kg,wioea in u$,w'ipe and all TCUP/SPLP extracts IA ug/L <br /> ND means not detecred above the reporting limit N/A nteaw analyte not applicable to this ainalysis <br /> (h)2-propanone or dimethyl ketone; (c)(2-chtoroethuxy)ethene; (d)2-h4=nooe;(c)dicbloron,ethanu;(f)2-butstnone; (g)4-:wthyl-2- <br /> pcntanone or isapmpylacertme; (h)lighter than water immiscible sheen 13 preFent;(i)liquid sample that contains greatm than-.5 vol,`Yo <br /> • sediment 6) sample diluted due lu high organic content; (k) ethenylbinyene; 1) metltylbenrenc; (m) acetic acid ethenyl es(rr: (n) <br /> chloroethane: o dimethylheTt es. <br /> DHS Certification No. 164-4 Edward Hamilton,Lab Director <br />