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• • <br /> CERTIFICATE OF ANALYSIS <br /> 8260B <br /> Report# R018-12 <br /> Sample ID: Stock Pile <br /> Lab ID: R200055 <br /> Method RL Analyte Results Units <br /> 8260B 5.0 Bromobenzene ND µg/Kg <br /> 5.0 Bromochloromethane ND <br /> 5.0 Bromomethane ND <br /> 5.0 n-Butylbenzene ND <br /> 5.0 sec-Butylbenzene ND <br /> 5.0 tert-Butylbenzene ND <br /> 5.0 Chloroethane ND <br /> 10 2-Chloroethylvinyl Ether ND <br /> 5.0 Chloromethane ND <br /> 5.0 2-Chlorotoluene ND <br /> 5.0 44Chlorotoluene ND <br /> 5.0 Dibromomethane ND <br /> 5.0 1,3-Dichlorobenzene ND <br /> 5.0 Dichlorodifluoromethane ND <br /> 5.0 1,3-Dichloropropane ND <br /> 5.0 2,2-Dichloropropane ND <br /> 5.0 1,1-Dichloropropene ND <br /> 5.0 Hexachlorobutadiene ND <br /> 5.0 Isopropylbenzene ND <br /> 5.0 p-Isopropyltoluene ND <br /> 5.0 Methyl tert-Butyl Ether(MTBE) ND <br /> 5.0 n-Propylbenzene ND <br /> 5.0 1,1,1,2-Tetrachloroethane ND <br /> 5.0 1,2,3-Trichlorobenzene ND <br /> 5.0 1,2,3-Trichloropropane ND <br /> 5.0 1,2,4-Trimethylbenzene ND <br /> 5.0 1,3,5-Trimethylbenzene ND <br /> 5.0 1,2-Dibromo-3-chloropropane(DBCP) ND <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% <br /> 1,2-Dichlorcethane-d4 20 18.9 94.50 66-133 <br /> 2-Bromo-l-chloropropane 20 23.9 119.50 63-139 <br /> 4-Bromofluorobenzene 20 15.1 75.50 64-136 <br /> ario DD'C)ixtofnO Donna Keller <br /> Chemist Certification #2585 Laboratory Director <br /> Page 2 of 2 <br />