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STL Seattle Blank Spike/Blank Spike Duplicate Report Lab ID: SWI 109 Date Prepared: 4/22/2005 Date Analyzed: 4/25/2005 QC Batch ID: SW1109 Semivolatile'Organics by USEPA Method 625 Blank Spike BS BSD Result Amount Result BS Result BSD Compound Name (ug/L) (ug/L) (uglL) %Rec: (ug/L) % Rec. RPD Flag Phenol 0 10 7.55 . 75.5 6.27 62.7 -19 bis(2-Chloroethyl)ether 0 10 8.42 84.2 7.95 79.5 -5.7 2-Chlorophenol 0 10 9.43 94.3 8.11 81.1 -15 1,3-Dichlorobenzene 0 10 9.92 99.2 8.65 86.5 -14 1,4-Dichlorobenzene 0 10 9.54 95.4 8.7 87 -9.2 1,2-Dichlorobenzene 0 10 11.5 115 10.5 105 -9.1 bis(2-Chloroisopropyl)ether 0 10 9.27 92.7 8.47 84.7 -9 N-nitroso-di-n-propylamine 0 10 10 100 8.62 86.2 -15 Hexachloroethane 0 10 8.46 84.6 8.34 83.4 -1.4 Nitrobenzene 0 10 10.3 103 10.7 1,07 3.8 Isophorone 0 10 8.64 86.4 9.4 94 8.4 2-Nitrophenol 0 10 9.12 91.2 6.74 67.4 -30 2,4-Dimethylphenol 0 10 8.86 88.6 9.8 98 10 bis(2-Chloroethoxy)methane 0 10 10.3 103 9.41 94.1 -9 2,4-Dichlorophenol 0 10 7.89 78.9 8.6 86 8.6 1,2,4-Trichlorobenzene 0 10 9.36 93.6 8.61 86.1 -8.3 Naphthalene 0 10 8.69 86.9 9.57 95.7 9.6 Hexachlorobutadiene 0 10 8.55 85.5 8.85 88.5 3.4 4-Chloro-3-methylphenol 0 10 9.05 90.5 9,03 90.3 -0.22 Hexachlorocyclopentadiene 0 10 7.08 .70.8 7.14 71.4 0.84 2,4,6-Trichlorophenol 0 10 11.2 112 10.9 109 -2.7 2,4,5-Trichlorophenol 0 10 8,18' 81.8 8.01 80.1 -2.1 2-Chloronaphthalene 0 10 9.13 91.3 8.54 85.4 -6.7 Dimethylphthalate 0 10 8.21 82.1 8.08 80.8 -1.6 Acenaphthylene 0 10 9.73 97.3 8.96 89.6 -8.2 2,6-Dinitrotoluene 0 10 8.21 82.1 8.83 88.3 7.3 Acenaphthene 0 10 9.56 95.6 8.79 87.9 -8.4 2,4-Dinitrophenol 0 10 6.99 69.9 6.44 64.4 -8.2 4-Nitrophenol 0 10 7.95 79.5 5.89 58.9 -30 Dibenzofuran 0 10 8.9 89 9.06 90.6 1.8 2,4-Dinitrotoluene 0 10 9.3 93 9.25 92.5 -0.54 Diethylphthalate 0.055 10 8.45 83.9 8.05 80 -4.8 4-Chlorophenylphenylether 0 1.0 9.46 94.6 8.31 83.1 -13 Fluorene 0 10 9.47 94.7 8.9 89 -6.2 4,6-Dinitro-2-methylphenol 0 10 9.41 94.1 9.29 92.9 -1.3 m m N