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Report Number 34755 4C Report Matrix Spike)Matrix Spike Duplicate Date 09/11/2003 Project Name PARMAR TEXACO Project Number Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Vafue Level Level Value Value Units Method Analyzed Recov Recov Diff Limit_-- Limit Benzene 34789-01 <0 0050 00374 00371 00317 00288 mg/Kg EPA 82608 916103 848 778 870 70-130 25 Toluene 34789-01 <0 0050 00374 00371 00286 00256 mg/Kg EPA 8260B 916103 764 690 103 70-130 25 Ter#-Butanol 34789-01 0 021 0187 0186 0151 0141 mg/Kg EPA 8260B 9/6103 693 643 743 70-130 25 Methyl-t-Butyl Ether 34789-01 0 086 00374 00371 0125 0116 mg/Kg EPA 8260B 916103 106 808 26 8 70-130 25 Benzene 34774-12 <0 50 400 400 423 412 ug/L EPA 82608 914103 106 103 256 70-130 25 Toluene 34774-12 <0 50 400 400 441 434 ug/L EPA 8260B 914103 110 108 169 70-130 25 Tert-Butanol 34774-12 <5 0 200 200 193 198 ug/L EPA 8260B 914103 963 989 267 70-130 25 Methyl-t-Butyl Ether 34774-12 <0 50 400 400 404 407 ug/L EPA 82608 914/03 101 102 0 764 70-130 25 Benzene 34793-08 <0 50 400 400 433 423 ug/L EPA 8260B 915103 108 106 236 70-130 25 Toluene 34793-08 <0 50 400 400 453 439 ug/L EPA 8260B 915103 113 110 325 70-130 25 Tert-Butanol 34793-08 <50 200 200 199 199 ug/L EPA 8260B 915103 997 995 0201 70-130 25 Methyl-t-Butyl Ether 34793-08 5 2 400 400 472 466 ug/L EPA 8260B 915103 105 103 149 70-130 25 Benzene 34786-01 <0 50 400 400 432 414 ug/L EPA 8260B 917/03 108 104 416 70-130 25 Toluene 34786-01 <0 50 400 400 450 435 ug/L EPA 82606 917103 112 109 334 70-130 25 Tert-Butanol 34786-01 83 200 200 210 206 ug/L EPA 82660B 9/7103 101 989 190 70-130 25 Methyl-t-Butyl Ether 34786-01 <0 50 400 400 419 413 uglL EPA 8260B 917/03 105 103 144 70-130 25 fl.on- 'D, JI KIFF ANALYTICAL, LLC Approved 8y `J 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800