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• ,/18/2005 09:01 2P 33433 EHD PAGE 00 <br /> 1MINIMUM VERIFICATION 1A80RATORY ANALYSIS <br /> TANK TANKTPl1•G TPH•D OXYGEN <br /> e CONTENTS 8015 DTX&E CL HC TOTAL MTBE <br /> 8015 $010 ✓1010 ATES KrTAt. PCC3 <br /> 8260 8260 8260 6240 7420D 8260 T�IPL•, ICAP/ 8270 <br /> 8260 7421 ETBL, ACS ar 8080 <br /> TAML••) AA <br /> LEADCD GAS X 1260 <br /> X X <br /> UNL GASX X <br /> X <br /> D1ESE1, X X <br /> X <br /> KEROSENE X X <br /> X <br /> UNK FUEL X X <br /> X X X <br /> PROD. OIL X X <br /> X <br /> CHLOR. <br /> SOLVENI'S 1 X X <br /> X <br /> NONCIiLOR <br /> SOLVENTS X X X <br /> WASTE\ <br /> USED OIL X X X <br /> X <br /> Al1analysls methods tut the designatedX X X <br /> Specifically noted below, described In EPA SW 846,Third poldon, 'those methods not found !n SW 846 are <br /> Refrr to the "SWRCB LUF'j'Field Manual",Appondix D 8 <br /> limits for motor vchJcic fuel (gasoline and diesol), Refer to "Tri-Regional Board Staff Rccomm'erndatlons for Initial Evaluation ana <br /> Investigation of US1`s' for the waste and motor oil minimum detection limlu, Uttecttoa)Limits that or Page <br /> A20 for minimum dctect;on <br /> AUowablc Limit of the contatnlnant in question will be accepted,however laboratory chill utdize theMost cons Ute MCL, STLC or <br /> ervativc method. <br /> TPH•G Total Pcnolewrt}lydrocarboll, Gasoline,GC/FID(50 0)1015 mod orEGC/1y�60OLOGYr <br /> ITH-D Total Petroleum Hydrocarbon,Dies{l, GC/FID(3550),8015 mod or GC/M$8260 <br /> i3TX& E} Acme,Toluene,Xylcne k Ethyl Benzcrte,GGPM 8020 orGC/MS 8260 <br /> CL HC Chloiaatcd l lydrocabon,OC/1-ISD 8010,GC/MS 8240 or 8260 <br /> 70'fAL LEAD l'oWl lead,AA 1420, AA 7421 or(CF-AES 6010 <br /> OXYGENATES )vg13E,ETBIr,TAME,D1PE,do TBA GC/1y5 8260(Tor MTBE <br /> MFTALS ICAP w AA Inducdvely Couplad Plusmo AtCC/)otric S 1260( or MTBE Liala my you may use 8 02 0) <br /> Cadmium,Chromium III"ad VI010 orAtomia Absorption Spcctranatry 7000. 'rsci„I$: <br /> PCH Poly chlorinated Biphenyls,GC/MS 8170 or 8080 'head,zine and NiNlekel. <br /> GC-FID Gas Chromatography,Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> Mctbod 3540 Soxhlct sample prep"tion <br /> Method 3550 Sonication sample preparuloa,extraction method <br /> 144hod 5030 Purge utd trap sample preparaUou <br /> QA./QC Quality Asavrunce/Quality Control <br /> No-Lc <br /> ackc' Ol avoid false positive detection of bcnzerse ben:anc•t}ec solvern�ye l0 be used. Fused capillary C0lulbns aro preferred to pocked columns a <br /> packed colurun may be used au a "fires cut"with'dirty'samples or Duca clic hydrucarboni have btca r�aracterized andproper A/Q <br /> drinking wafer tanras,EPA rrcomrnestdy shat clic 500 attici for voluUle <br /> lin nr arc lower or2ianie tbould be Wed in pl char ct to the 600 eQA/QC itl f dctcc d, For <br /> and the QA/QC is better. Samples c dtibiting any Ievcl of heavy rectal cootarnlnation may require further an <br /> furtheralyst+,pHS.E� <br /> rmorrunendi 1w010'ng Nuse samples until d4osaJ is indicated. <br /> H 23 046 (Revised 05/09/00) <br /> 5 <br />