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C <br /> ,/18/2005 09:01 2P 93433 END PAGE 06 <br /> MINIMUM VERIFICATION LABORATORY ANALYSIS <br /> TANK TANKTPH G TPH•D OXYt3EN <br /> e CONTENTS TPH DTX do E CL HC TOTAL MTBE <br /> 8015 $020 $010 AWES '^u PC3 <br /> 8020 ( <br /> 8260 8260 $260 8240 7420D $260 TS IP 1-:1 ICAP/ 8270 <br /> 8260 7421 ETBL, ACS or 8080 <br /> TAME) AA <br /> LEADCD GAS X 1260 <br /> X X <br /> UNL GASX X <br /> X <br /> D1ESE1, X <br /> X X <br /> KEROSENE X X <br /> X <br /> UNK FUEL X X <br /> X X X <br /> PROD. OIL X X <br /> X <br /> CHLOR. <br /> SOLVEMPS X X <br /> X <br /> NONCHLOR _ <br /> SOLVENTS X X X <br /> WASTE\ <br /> USED OIL X X X <br /> X <br /> A11artslysls methods ter the designatedX X X <br /> specilically noted below, EPA methods described in EPA SW 846,Third Edition, Those methods not found Jn SW 846 are <br /> Refrr to the "SW1tCB LUFI'Feld Manual" <br /> limits for motor vthlcic fuel (Sasolint and diesol). Rcfer to "Tri-Rogiona) Board Staff Rccomm'endatlons for Initial Evaluation ane <br /> InvesciYation of US1's" for tho waste and motor oil minimum detection litnits.ollKandix �loo)L able 3•S on paSe A20 for minimum d�tea,on <br /> AUowxblt Limit of the eontatnJAM In question will be accepted,however laboratory iballJut[1Jze themostbe low Wtr,tM L,STL <br /> h dC or <br /> TPH•G Total Perro)eurn tlydrocvbotl, Gasoline, AI30-I(SO 0)i015 mod SESor TZRIM60OLOGY: <br /> 1 -X& Tota)➢clroleunl hydrocarbon,Diesel,GC/FID(3550),8015 mod or GC/MS 8260 <br /> CL DTH do cl3erucne,Tolutn o Xylene dc Edtyl Banzerte, GC/PM 8020 or GC/M5 8260 <br /> TOA Chloro°tad hylead, bon,GC/FISD$010,GC/MS 8240 or$260 <br /> 70'fAl.LEAD 1'ou,l ItatJ,AA 7420, AA 7421 or(CF-AES 6010 <br /> OXYGENATES VIBE,ETBZ,TAME DLIE &T8A G <br /> MITA-S ICAP w AA CSS$260(Tor MTBE <br /> OC/)4S Coupled Plusmo Atonic Ernisalon Specu,=cvy 60 my You may use 8020) <br /> Cadmium,Chromium(I1 and VI h 6010 orAtomio Absorption Spectranetry 7000. Marls: <br /> PCH Polych)orinatcd Bi*nyb,GC/MS 8270 or Soto Lead'Zine and Nickel. <br /> OC•F1D Gat Chromatography,Flame Ioniration Defection <br /> lvtcrhod 3030 Acid digestion <br /> Mctbod 3 N Soxhlct sample pnipanition <br /> Method 3330 J'oniation sample Prq=,40111,extraction method <br /> Mothod 5030 Purge and trap sample prryaretlon <br /> QA/QC Quality Autwnce/Qwjity Control <br /> No. ! To avoid fa)sc positive detection of benzene,bcntCnc•troe solvtmts arc to be used. Fused capil)ary Calufnni era praferred to Pinked wlurnns a <br /> packed column may be used m a "first cut•with°dirty"samples or oiled[hc hydrocarbons kava been rhsraotaizcd andProper A/ <br /> d1Lnk- 9 water—I ccs,EPA rccommends that the 500 aeries for volutlle orbanle should tea <br /> lin us arc)ower usd the AJ Q QC is followed, For <br /> Q QC)c butts!. Samples CChibiticd any leve(ofhepYy mCtal COO&Mlnatio meay require further eirnal si.j pHs E�tcction <br /> recomntnds holding those samples until disposal is indicplcd. <br /> EH 23 046 (Revised 05/09/00) <br /> 5 <br />