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io <br /> Sequoia 680 Chesapeake Drive Redwood City CA 94063 (650)364-9600 FAX(650)364 9233 <br /> 404 N Wiget Lane Walnut Creek.CA 94598 (925)988-9600 FAX(925)988-9673 <br /> Analytical 819 Striker Avenue Suite 8 Sacramento CA 95834 (916)921-9600 FAX(916)921-0100 <br /> 1455 McDowell Blvd North Ste D Petaluma,CA 94954 (707)792-1865 FAX(707)792-0342 <br /> • <br /> Cambna Environmental Project Shell Oil Co Sampled 1/14/99 to 1115/99 <br /> 270 Perkins St Project Number 880 Victor Rd-Lodi Received 1118199 <br /> Sonoma,CA 95476 Project Manager Aubrey Cool Reported 1128199 <br /> Volatile Organic Compounds by EPA Method 8260B <br /> Sequoia Analytical-Petaluma <br /> Batch Date Date Surrogate Reporting <br /> AnaEyte Number Prepared Analyzed Lirruts Linut Result Units Notes* <br /> SB-1-25 0' P901240-05 Soil <br /> Tert-amyl methyl ether 9010445 1125199 1/26/99 20000 ND ug/kg <br /> Tert-butyl alcohol " 11 400000 ND " <br /> Di-isopropyl ether It <br /> 20000 ND " <br /> Ethyl tert-butyl ether 20000 ND " <br /> Methyl tert-butyl ether 4000 92900 " <br /> Surrogate Dibromofluoromethane 800-120 ND % 2 <br /> Surrogate 12-Dichloroethane-d4 800-120 ND 2 <br /> Surrogate Toluene-d8 810-117 ND 2 <br /> Surrogate 4-Bromofluorobenzene 740-121 ND 2 <br /> SB-1-35 0' P901240-07 Sail <br /> Tert-amyl methyl ether 9010445 1125199 1/25/99 2000 ND ug/kg <br /> Tert-butyl alcohol 40000 ND " <br /> Di-isopropyl ether 2000 ND <br /> Ethyl tert-butyl ether 2000 ND " <br /> Methyl tent-butyl ether 400 15000 " <br /> Surrogate Dibromofluoromethane 800-120 970 % <br /> Surrogate 12-Dichloroethane-d4 800-120 104 " <br /> Surrogate Toluene-d8 810-117 950 " <br /> Surrogate 4:Bromofluorobenzene--- '-- "-- - 74 0=121-- T_ 105 - <br />__ _SB-1=40 5' - - P901240-08 - - ----- _ — Soil. <br /> Tert-amyl methyl ether 9010445 1/25199 1125199 1000 ND ug/kg <br /> Tert-butyl alwhol - - 20000 ND " <br /> Di-isopropyl ether 1000 ND " <br /> Ethyl tert-butyl ether 1000 ND " <br /> Methyl tert-butyl ether 200 1090 " <br /> Surrogate Dibromofluoromethane 800-120 102 % <br /> Surrogate 1 2-Dichloroethane-d4 800-120 109 <br /> Surrogate Toluene-d8 to810-117 995 <br /> Surrogate 4-Bromofluorobenzene " " " 740-121 110 " <br /> SB-2-35 0' P901240-14 Soil <br /> Tert-amyl methyl ether 9010445 1/25/99 1/26/99 1000 ND ug/kg <br /> Tert-butyl alcohol 20000 ND " <br /> Di-isopropyl ether 1000 ND " <br /> Ethyl tert-butyl ether 1000 ND " <br /> Methyl tert-butyl ether 200 1760 <br /> Surrogate Dibromofluoromethane 800-120 '102 % <br /> Surrogate 1 2-Dichloroethane-d4 to800-120 93 5 " <br /> Surrogate Toluene-d8 810-117 114 or <br /> Sequoia Analytical-Petaluma *Refer to end of report for text of notes and definitions <br /> Page 7 of 20 <br />