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03/12/98 TIFU 11:10 FAX 7077920342 PASILod <br /> f]013 <br /> Pace Analytical Services,Inc. <br /> ti r 1455 McDowell Blvd.North,Suite D <br /> Pace An lytical Petaluma,CA 94954 <br /> Tel:707-792-1865 <br /> i F :707-792-0342 <br /> QUALITY CONIROL DATA DATE: 03112/ <br /> PAGE: 3 <br /> I <br /> `r <br /> s <br /> ERM WEST. Inc. Pace Project Number: 7010822 <br /> 1777 Botelho Or Client Project ID: Heinz-Tracy <br /> s: Suite 260 SDG !Number: 7010922 I <br /> ;{ Walnut Creek, CA 94596 <br /> { Attn: Mr. Carl Von Stetten <br /> Phone: (510)446-0455 I <br /> QC Batch ID: 31893 QC Batch Method: EPA 3050 <br /> Analysis Method: EPA 6010 Analysis Description; Metals, ICP <br /> Associated Pace Samples: 701284739 <br /> °-0 MEl}tQD BLANK: 701285207 I <br /> y Associated Pace Samples: <br /> f=�a <br /> 701284739 <br /> Method <br /> Blank <br /> Parameter Units Result PRL Footnotes <br /> ....... ... i <br /> Cadmium mg/kg ND 0.5 <br /> Chromium mg/kg NO 0.7 <br /> Y <br /> Lead <br /> mg/kg ND 5 <br /> Nickel mg/kg NO 3 <br /> Zinc mg/kg NO 2 <br /> MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 701285215 701285223 Matrix Matrix Spike <br /> Spike Spike Spike Sp. Dup. Dup <br /> Parameter Units 701284739 Conc. Result X Rec Result X Rec RPD Footnotes <br /> --------------- ..... .......... .......... ....... .......... ..... - j <br /> Y Cadmium <br /> mglkg 0.4762 4.1 3.865 83.4 3.877 90.5 8 ! <br /> Chromium mg/kg 24.60 40.65 61.80 91.5 56.47 84.8 6 <br /> { Lead mg/kg 11,02 40.65 44.07 81.3 46.59 94.6 15 <br /> Nickel mg/kg 28.36 40.65 .67.63 96.6 59.9D 63.9 14 <br /> Zinc mg/kg 95.88 40.65 125.9 73.7 197.3 270 114 1 <br /> 1; <br /> :- LABORATORY CONTROL SAMPLE: 701285231 <br /> Spike LCS Spike <br /> Parameter Units Conc. Result t Rec Footnotes <br /> ------------------------------ .......... ......• ---------- <br /> Cadmium mg/kg 5.0 5.277 106 <br /> Chromium mg/kg 50 49.61 99.2 <br /> Lead mg/kg 50 48.66 97.3 <br /> i <br /> y� I <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except In full, <br /> without the written consent of Pace Analytical Services,Inc. <br /> l: <br />