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= IM ir Report Number 31607 QC Report Matrix Spike/Matrix Spike Duplicate Date 02/27/2003 Protect Name Stefano's Protect Number Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Vaiue Units Method Analyzed Recov Recov Diff Limit Limit Benzene 31624-04 <0 50 399 400 406 400 ug/L EPA 82606 2122103 102 100 1 86 70-130 25 Toluene 31624-04 <0 50 399 400 407 400 ug/L EPA 82606 2122103 102 100 1 78 70-130 25 Tert-Butanol 31624-04 17 200 200 212 210 ug/L. EPA 82606 2122103 97 6 96 3 1 38 70-130 25 Methyl-t-Butyl Ether 31624-04 <0 50 399 400 347 35 5 ug/L EPA 82606 2122/03 870 886 191 70-130 25 Benzene 31621-01 <0 50 400 400 366 36 5 ug/L EPA 82608 2121103 91 6 914 0 219 70-130 25 Toluene 31621-01 <0 50 400 400 355 35 6 ug/L EPA 82606 2121103 887 89 0 0 310 70-130 25 Tert-Butanol 31621-01 <5 0 200 200 194 197 ug/L EPA 8260B 2121103 972 985 136 70-130 25 Methyl-t-Butyl Ether 31621-01 34 400 400 41 0 410 ug/L EPA 8260B 2121103 94 2 941 00531 70-130 25 Benzene 31614-05 <0 50 400 400 379 374 ug/L EPA 8260B 2121103 94 7 935 1 33 70-130 25 Toluene 31614-05 <0 50 400 400 37 7 383 ug/L EPA 8260B 2121103 944 958 152 70-130 25 Tert-Butanol 31614-05 <50 200 200 192 190 ug/L EPA 82606 2/21103 958 951 0 760 70-130 25 Methyl-t-Butyl Ether 31614-05 20 400 400 51 1 51 0 ug/L EPA 82606 2121103 778 777 00965 70-130 25 Benzene 31613-01 083 400 400 39 9 39 5 ug/L EPA 8260B 2121103 976 96 7 0 875 70-130 25 Toluene 31613-01 13 400 400 408 404 ug/L EPA 82606 2121103 98 7 979 0 839 70-130 25 Tert-Butanol 31613-01 <5 0 200 200 208 203 ug/L EPA 8260B 2121103 104 101 262 70-130 25 Methyi-t-Butyl Ether 31613-01 7 9 400 400 464 461 ug/L EPA 82606 2121103 961 954 0 757 70-130 25 Approved By J QI Kiff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800