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819 Striker Avenue,Suite8 Sequoia Sacram958 ' ento, 34 (916)92 9561-9600 FAX(916)921-0100 ' TOWAnalytical www.seciuolalabs.com ' Kleinfelder-Stockton Project: Helena Chemical 2825 East Myrtle Street Project Number: 23-0850-60 Reported: Stockton CA,95205 Project Manager: Joe Zilles 04/22/02 13:14 ' Conventional Chemistry Parameters by APHA/EPA Methods Sequoia Analytical- Sacramento Reporting Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes 25000-B1-6"(5204095-01)Soil Sampled:04/03/02 09:45 Received:04/04/02 08:15 Ammonia as N 5.5 5.0 mg/kg 1 2040126 04/09/02 04/12/02 EPA 350.3 25001-B1-1 1/2'(S204095-02)Soil Sampled:04/03/02 09:45 Received:04/04/02 08:15 'Ammonia as N ND 5.0 mg/kg 1 2040126 04/09/02 04/12/02 EPA 350.3 25004-B2-6"(5204095-05)Soil Sampled:04/03/02 09:55 Received:04/04/02 08:15 Ammonia as N ND 5.0 mg/kg 1 2040126 04/09/02 04/12/02 EPA 350.3 25005-B2-1 1/2'(S204095-06)Soil Sampled:04/03/02 09:55 Received:04/04/02 08:15 Ammonia as N 7.5 5.0 mg/kg 1 2040126 04/09/02 04/12/02 EPA 350.3 25008-B3-6"(S204095-09)Soil Sampled: 04/03/02 10:10 Received:04/04/02 08:15 Ammonia as N 19 5.0 mg/kg 1 2040126 04/09/02 04/12/02 EPA 350.3 25009-B3-1 1/2'(S204095-10)Soil Sampled:04/03/02 10:10 Received:04/04/02 08:15 'Ammonia as N 26 5.0 mg/kg 1 2040126 04/09/02 04/12/02 EPA 350.3 250012-1114-6"(S204095-13)Soil Sampled:04/03/02 10:20 Received:04/04/02 08:15 'Ammonia as N 450 5.0 mg/kg 1 2040126 04/09/02 04/12/02 EPA 350.3 25013-B4-1 1/2'(S204095-14)Soil Sampled:04/03/02 10:20 Received:04/04/02 08:15 Ammonia as N 2500 5.0 mg/kg 1 2040171 04/15/02 04/15/02 EPA 350.3 250016-B5-6"(S204095-17)Soil Sampled: 04/03/02 10:35 Received:04/04/02 08:15 'Ammonia as N 10 5.0 mg/kg 1 2040171 04/15/02 04/15/02 EPA 350.3 Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. r Page 4 of 24