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819 Striker Avenue,Suite 8 <br /> ' Savamento.16 92 95834 <br /> -9600 <br /> Sequoia (916)921-9600 <br /> FAX(916)921-0100 <br /> `, V Analytical vvvvvv.seguolaiabs.com <br /> [2825 <br /> nfelder-Stockton Project: Helena Chemical <br /> East Myrtle Street ProjectNumber: 23-4850-60 Reported: <br /> kton CA,95205 Project Managa: Joe Zilles 04/22/02 13:14 <br /> Conventional Chemistry Parameters by APHA/EPA Methods- Quality Control <br /> Sequoia Analytical- Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %BEC Limits RPD Limit Noles <br /> Batch 2040198-General Preparation <br /> ILCS(2040198-BSI) _ _ Prepared&Analyzed:04/17/02 <br /> Ammonia as N 4270 5.0 mg/kg 4110 104 80-120 <br /> Matrix Spike(2040198-MSI) Source:S204095-61 Prepared&Analyzed:04/17/02 <br /> Ammonia as N 3940 5.0 mg/kg 4110 ND 95.9 75-125 <br /> fMatrix Spike Dup(2040198-MSDI) Source:S204095-61 Prepared&Analyzed:04/17/02 <br /> mnonia as N 3940 5.0 mg/kg 4110 ND 95.9 75-125 0.00 20 <br /> i <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. This analytical report must be reproduced in its entirety. <br /> Page 20 of 24 <br />