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McCarnpbell Analytical Inc 11°211d A--SO1th+#A7 Pasco,CA 94553-5560 <br /> Telephone 92S-798-1620 Fax 925-798-1622 <br /> h Jlwww bell cam 8-m it nT@TXan#xIIcoin <br /> - _ FShaw <br /> oEnvlronmental,Inc Client Project ID Geweke <br /> - � Date Sampled _ 12/23/02 <br /> ad Date Received12/26/02 <br /> Stockton,CA 95215 Client Contact Bob Marty Date Extracted 12/26/02-12/28/02 <br /> Client P O Date Analyzed 12/26/02-12/28/02 <br /> Volatiles Organics by P&T and GC/MS(Basic Target List)* <br /> Eicdactraa Method SW5030B Aualyacal Method, SW8260B <br /> -. Work Order 0=4w <br /> ID 0212409-011$ <br /> Client ID MWl l <br /> Matrix Water <br /> Acetone <br /> Compound Concentration " DF las Corimund Conceritratton DF , <br /> NDC20 to 50 Benzene <br /> Bromoberizene ND ID 05 Brnrnwhloramethane ND 10 0 5 <br /> Bromodichloromethane ND 10 0 5 Bromofotm ND to 0.5 <br /> Bmmomedume ND 10 0 5 2-Butanone F-K ND 10 0 5 <br /> n-Bu benzene ND 10 05 sec_Buz 1 0 1 0 <br /> tort-Bu 1 benzene ND 10 05 Carbon Disulfide ND 10 05 <br /> Carbon Tetrachloride ND 1 0 0 5 Chlorobenzene ND 10 05 <br /> Chloroethane ND 1 0 0 5 2�1t1oroethVtn I Ether ND 10 0 5 <br /> Chloroform ND ND 1 0 0 5 <br /> 2 Chlorotoluene _ <br /> 1 0 0 5 Chloromethane ND 1 0 0 5 <br /> ND 1 0 05 4-Chlorotoluene <br /> Dibromochloromethane ND ]0 05 1,2-Dtbromo-3-ch1 a ND 1 ND 1 0 05 <br /> 1,2-Dtbromoedianc EDB ND to 05 Dibromomathaae 0 0 5 <br /> 1,2-Dichlorobenzene ND 10 0 5 1,3-Dichlorobenzene ND 1 0 0 5 <br /> ND 10 05 <br /> 1,4-Dichlorobenzene ND 1 0 05 Dichlorodi8tioromethane <br /> 1,1-Dichloroethane ND [0 05 1,2-Dichlorixthane 1,2-DCA ND 1 0 O S <br /> 1,1-Dichloroethene ATDS 0 84 1 0 0 5 <br /> tr <br /> 1 0 0 5 thene cis-1,2-DichloroeND l 0 0 5 <br /> 1,3-Dichloroa ans-I,2-1,2ND ] 0 0 5 1,2-Dtchloro a NQ 10 05 <br /> ND 10 0 5 2,2_Qichloro ane <br /> 111-Qtchloroa ND 10 0 5 cis-I,3-Dtchloro a ND to 05 <br /> trans-l,3-Dichlororo a ND 10 0 5 Eth lbenririe ND 1 0 0 5 <br /> ND 10 0 5 <br /> Flexachlorobutadiene <br /> ND 10 0 5 2-Hexanone ND 1 0 0 5 <br /> Iodomethane eth 1 iodide ND 1 0 1 0 4-Iso ro I toliiene <br /> Iso r° (benzene ND [0 05 4-Meth i-2 none 1BlC ND 1 0 0 5 <br /> methylene chloride ND 1 0 0 5 <br /> ND 1 0 0 5 Meth I-t-bu I ether MTBE <br /> ND 10 05 <br /> Naphthalene ND 10 05 n-Pro benzene <br /> S e ND 10 05 1,],1,2-Tetrachloroethane ND 10 05 <br /> 1.1,2,2-Tetrachloroethane ND 10 0 5 TetrachloroND 1 0 0 5 <br /> ethene ND to 0 5 <br /> Toluene ND 10 05 1,2,3-Tnchlorobenzene <br /> 1,24-Tnchlorobenzene ND to 0 5 111,1-Tnehloroethane ND 10 05 <br /> 1,I,2-TrichloroethaneND 10 0 5 Trichloroethene No1 0 0 5 <br /> Tnchlomvfluoromethane ND l 0 0 5 <br /> 1,2,4-Tnm5LA lbenzene ND 1 0 0 5 I,2,3-Tnchloro a ND 10 05 <br /> Vinyl Acetate <br /> ND I 0 o5 zen <br /> 1,3,5-Tnmeth lberte ND 1 0 0 5ND 10 50 Vin 1 Chloride <br /> Xylenes ND 1OS ND to 05 <br /> 0 <br /> %SSl Surrogate Recoveries(•/,) <br /> 108 <br /> %SS3 98 6 %SS2 8 <br /> Comments <br /> "water and vapor samples and all TCLP&SPLP extracts are reported mµg/i„soilksludgelsolid sam les m <br /> product/oiUnon-aqueous liquid samples in mg/L. P lig/kB. wipe samples in jig/wipe, <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> h)11 ghter than water immiscible sheen/product is present,i)liquid sample that eontams greater than--2 vol orb sediment,l)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />