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t S <br /> � r <br /> _r McCampbell Analytical Inc10�"d A"en1e 1+#m Pachmo CA 94553-5560 <br /> Telephone 923-798-1620 Fax 925-798-1622 <br /> hnpJ/www mccampbell com E-mail mam(a�mccampbeil xm <br /> i L <br /> QC SUMMARY REPORT FOR SW87.60B - <br /> Matmt W WorkOrder 0212409 <br /> EPA Method SM260B Extraction SW5030B <br /> BatchfD 5449 Spiked5ampleiD 0212409-0118 <br /> Compound Sample Spiked MS' MSD' MS-MSD' LCS LCSD LCS-LCSD Acceptance Cntena(%) <br /> N9/L P9/L %Rec. %Rea %RPD %Rec %Rea %RPD Low ---High <br /> cert-Amyl methyl ether(TAME} ND 10 102 102 0 576 925 932 0 731 70 I30 <br /> Benzene ND to 112 114 156 105 105 0160 <br /> 70 130 <br /> DirsoPrnpyl ether(D1PE) ND 10 115 115 0 409 110 111 0 230 70 130 <br /> Ethyl cert-butyl ether(ETBE) ND 10 119 120 0 927 113 113 4 490 _ µ <br /> 70 130 <br /> Methyl-t-butyl ether(MTBE) ND 10 114 115 0 973 -104 _--- <br /> 105 0 307 70 130 <br /> Toluene ND 10 115 117 171 115 116 0 742 70 Y 130 <br /> "/aS'S 1 108, 100 113 114 120 785 761 3 14 7d <br /> 130 <br /> %SS2 998 100 10l 101 0 477 105 106 0946 70 v T <br /> 130 <br /> °/aSS3 1986 L00 97 1 % 1 15 I05 108 2 92 70 <br /> I30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following ex <br /> NONE ceptions <br /> r- <br /> r <br /> MS=Matrix Socks MSD=matrix Spike Duplicate LCS=Laboratory Control Sam <br /> De+reatron ole.LCSD=t ab=Wry Contra Sample Duplkate,RPD=Reia#w Peccant <br /> NIA=not enough aampie to perform matrix spike and malra spike duptkte <br /> NR=artaiyta concentration in sample exceeds spike amount for sod matrix or exceeds 2r spike amount for water matrix or sample diluted due to high matrix or <br /> anayEe content, <br /> %Recovery=100*(MS-Sample)/(Amount Spiked).RPO=100'(MS—MSD)/(MS+MSD) <br /> -2 <br /> 'MS and/or MSD spike reo0vedes may not be near 100%or the RPDs near 0%it a the <br /> analyte relabve to the amount spiked orb)of that spedfk;sample matnc�interfe y s serttple ie lnhorrfogernpciaANDeontains signefrcant wncaritratlans of <br /> Price re0overy <br />