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McCampbell Analytical Inc - 110 20d A--sO�aD7,Pacheco,CA 94553-5560 <br /> Tetephow 925-798-1620 FU 925-798-1622 <br /> - J/www p con Umail ca !Ecom <br /> .�. Advanced GeaEnvtronmental,Inc Client Project ID Geweke <br /> _ _ Date Sampled 12/23/02 _ <br /> 837 Shaw Road Date Received 12/26/02 <br /> Stockton,GA 95215 Client Contact Bob Marty Date Extracted 12/26/02-12/28/02 <br /> Client P O - Date Analyzed 12/26/02-12/28/02 <br /> Volatiles Orgarmes by P&T and GC/M3(Basic Target List)* <br /> Ex6aet<oaMethod SW503UB AnniyticWMcdKKL SW8260S <br /> Work Order 0212409 <br /> Lab ID 0212409-0048 <br /> Client ID MW4 <br /> Matrix Waxer <br /> Corimaund <br /> Acetone Concentration * DF Compound Concentr=an* DF r <br /> NDc20 10 50 Benzene <br /> Bromobonzene ND1 0 05 Bhlaromethane 061 I 0 0 5 <br /> romoc <br /> Bromodichlororricthane ND 10 0 5 Bromoform ND 10 05 <br /> Bromomethane ND 10 05 2-ButanoneEK ND 10 05 <br /> n-Bu benzene ND 10 0 5 see-Butyl benzene ND 10 10 <br /> tent-Bu benzene ND 10 0 5 <br /> ND 10 05 Carbon Disulfide <br /> Carbon Tetrachloride ND to 01 Chlorobenzene ND 1 0 0 5 <br /> Chloroethane ND 10 0 5 2-Chloroeth Vi1 Ether ND 10 0 5 <br /> Chloroform ND n 1 0 0 5 Chloromethane ND to 05 <br /> 2-Chlomtoluene NDE 0 0 5 4-Chlorotoluene ND 1 0 05 <br /> thbromochlorom (K ND 1 0 0 5 1,2-Dibromo-3�hloro ro e ND 10 0 5 <br /> 1,2-Dibromoethana 8 ND 10 05 <br /> ND 10 05 Dtbromomethane <br /> 1,2-Dichlorobenzene ND 10 0 5 1,3-Dichlorobenzene ND 1 4 0 5 <br /> 1,4-Dichlorobenzene ND 1 0 0 5 Dichlorodifluoromethane ND 10 05 <br /> III-Dichlomethane ND !0 O S i,2-Dtchlonoeth'ane 1anc ND 1 0 05 <br /> !,1-Dichloroethcne NO 10 0 5 16 l 0 4 5 <br /> trans-l,2-Dichlorocthene ac>s-l,2-Drchloroetheie ND 10 0 5 <br /> ND to 0 5 1,2-Dichloro a ND 10 05 <br /> 1,3-131chlo a ND 10 0 5 2,2-Dichloro ane <br /> I,l-Dtchlom a ND 10 0 5 cis-1,3-Diehl ND ! 0 05 <br /> trans-l,3-Drotchloroe e ND 1 0 0 5 <br /> ND 10 O S Eth benzene Hexachlorobutadiene ND 10 05 2-Hexanone ND ! 4 05 <br /> lodomethane eth I iodide ND I Q 10 4-kn itoluene ND 1 0 0 5 <br /> !benzene ND 10 0 5 4-Meth 1-2 tan' a M ND 1 0 0 5 <br /> Meth lene chloride ND ND 1 0 05 <br /> N hthalrne <br /> 10 0 5 Meth l-t-bu I ether MTBE ND 10 0 5 <br /> ND 10 0 5 ii-Propyl benzene <br /> Styrene ND 1 0 0 5 1,1,1,2-Tetrachloroethane ND 1 0 0 5 <br /> 1etrachloroediane ND 1 0. 0 5 Tetrachloroethene ND 1 0 0 5 <br /> Toluene ND 1 0 0 5 <br /> 1,2,4-Tnehlorobenzene ND 10 0 5 1,2,3-Tnchlorobenzene ND 1 0 0 5 <br /> 1 1,2-Trichloroethane <br /> ND 10 0 5 1,1,1-Trichloroethane ND 1 0 0 5 <br /> , ND 10 0 5 Trichloroethene <br /> Tnchlorofluoromethane ND 10 0 5 rich Tnchla a ND ! 0 0 5 <br /> VinylTnmete !benzene ND i 0 0 5 1,3,5-Tnmeth !benzene ND 1 0 0 5 <br /> Vin I Acetate ND Z O S 0 Vinyl Chloride ND L 0 0 5 <br /> X ]encs ND I D 0 ND I O 0 5 <br /> Surrogate Recoverfes(%) <br /> 44SS 1 Ito <br /> %SS3 95 5 %SSZ 985 <br /> Comments <br /> "water and vapor samples and all TCLP&SPLP extracts are it posted in <br /> product/otl/non-aqueous liquid samples in mg/L AV[,soil/sludgdsoiid samples in pg/kg, wipe samples inµg/wipe, <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than-.2 vol %sediment,J)sample diluted due to high <br /> oigansc content <br /> DHS Certification No 1644 <br /> Edward Hamilton,Lab Director <br />