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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-795-1620 Fax 925-798-1622 <br /> h //www mccam bell cam E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Geweke Date Sampled 03/18/2002 <br /> 837 Shaw Road Date Received 03/19/2002 <br /> Stockton,CA 95215 Client Contact Brian Millman Date Extracted 03/21/2002 <br /> Client P O Date Analyzed 03/21/2002 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 0203321-001 <br /> Client 1D EW1/031802 <br /> Matrix W <br /> Compound Concentration* RepGrung l'mr Compound Concentration* Rcpa mng LiTntt <br /> W S W S <br /> Acetone f ND 50 25 trans-1,3-Dichloropropene ND 10 50 <br /> Benzene ND 1 0 5 0 Ethylene dibrotrnde ND 10 50 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 10 5 0 <br /> Bromochloromethane ND 10 5 0 Hexachlorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 10 5 0 <br /> Bromoform ND 1 0 5 0 Isopropylbenzene ND 10 50 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 10 5 0 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride` ND 10 5 0 <br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 1 0 5 0 Methyl isobutyl ketone ND 1 0 50 <br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) ND 1 0 5 0 <br /> Chlorobenzene ND 1 0 5 0 Naphthalene ND 5 0 25 <br /> Chloroethane ND<5 0 to 5 0 n-Propyl benzene ND 1 0 5 0 <br /> 2-Chloroethyl Vinyl Ether` ND 1 0 5 0 Styrene MND 10 50 <br /> Chloroform ND 1 0 50 1,1,1,2-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND l0 50 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 1 0 50 <br /> 4-Chlorotoluene ND 10 50 Toluene ND 1 0 5 0 <br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-13ibromo-3-chloropmpane ND 20 10 1,2,4-Trichlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 10 5 0 <br /> 1,2-Dichlorobenzene ND 1 0 5 0 1,1,2-Tnchloroethane ND 10 5 0 <br /> 1,341ichlorobenzene ND 1 0 50 Trichloroethene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 10 50 <br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Tnchloropropane ND 10 5 0 <br /> 1,1-Dichloroethane ND 1 0 50 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 1 0 50 1,3,5-Tnmethylbenzene ND 10 5 0 <br /> 1,1-Dichioroethene ND 1 0 50 Vinyl Acetate m ND 5 0 25 <br /> cis-1,2-Dichioroethene ND 1 0 50 Vinyl Chlonde ° ND 10 5 0 <br /> trans-1,2-Dichloroethene ND 1 0 50 Xylenes,total ND 10 5 0 <br /> 1,2-Dichloropropane ND I 0 50 Comments <br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 98 <br /> 1,1-Dichloropropene ND 10 5 0 Toluene-d8 94 <br /> cis-1,3-Dichloropropene ND 1 0 50 4-Bromofluorobenzene 88 <br /> `water and vapor samples are reported in ug/L.,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e)dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquld sample that contains greater than—5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />