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0 7 <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//Wwwrnccannpbcllcorn E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Geweke Date Sampled 03/18/2002 <br /> 837 Shaw Road Date Received 03/19/2002 <br /> Stockton,CA 95215 Client Contact Brian Millman Date Extracted 03/21/2002 <br /> Client P O Date Analyzed 03/21/2002 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 0203321-003 <br /> Client ID MW2/031802 <br /> Matrix W <br /> Compound Concentration* Rcporung Lunt Compound Concentration* RepOrn Umit <br /> W S W S <br /> Acetone ) ND 50 25 trans-1,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 10 5 0 Ethylene dibromide ND 10 50 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 10 50 <br /> Bromochloromethane ND 1 0 1 5 0 Hexachlorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND 1 0 5 0 Iodomethane ND 10 50 <br /> Bromoform ND 1 0 50 Isopropylbenzene ND 1 0 5 0 <br /> Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND 1 0 5 0 <br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 1 0 5 0 <br /> sec-Butyl benzene ND 1 0 5 0 Methylene Chlonde° ND 1 0 50 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone ND 10 50 <br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) ND 1 0 5 0 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 5 0 25 <br /> Chloroethane ND<5 0 1 0 5 0 n-Propyl benzene ND 1 0 5 0 <br /> 2-Chloroethyl Vinyl Ether"' ND 1 0 50 Styrene W ND 1 0 50 <br /> Chloroform ND 1 0 5 0 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 1 0 50 <br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachlomethene ND 1 0 5 0 <br /> 4-Chlorotoluene ND 1 0 5 0 Toluene ND 1 0 50 <br /> Dibromochloromethane ND 1 0 50 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1 2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25 <br /> Dibromomethane ND 1 0 5 0 1,1,1-Tnchloroethane ND 1 0 5 0 <br /> 1,2-Dichlorobenzene ND 1 0 50 1,1,2-Tnchloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Trichlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnehloropropane ND 1 0 5 0 <br /> 1,1-Dichloroethane ND 1 0 50 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Tnmethylbenzene ND 10 50 <br /> 1,1-Dichloroethene ND 1 0 50 Vinyl Acetate M-1 ND 50 25 <br /> cis-1 2-Dichloroethene ND 1 0 5 0 Vinyl Chloride ° ND 1 0 5 0 <br /> trans-1,2-Dichloroethene ND t 0 5 0 Xylenes,total ND 1 0 so <br /> 1,2-Dichloropropane ND 10 5 0 Comments <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 98 <br /> l,l-Dichloropropene ND 1 0 5 0 1 Toluene-d8 94 <br /> cis-1,3-Dichloropropene ND 1 1 0 150 1 4-Bromofluorobenzene 86 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c)(2-chloroethoxy)ethene, (d) 2-hexanone, (e)dichloromethane, (1)2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol % <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />