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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> WCAMPBELL ANALYTICAL INC Telephone 925-7-98-1620 Fax 925-798-1622 <br /> http//wwwmccgMpbellcorn E-mail main@mccampbell com <br /> Advanced GeoEnvironnzental Client Project ID Geweke Date Sampled 03/18/2002 <br /> 837 Shaw Road Date Received 03/19/2002 <br /> Stockton, CA 95215 Client Contact Brian Millman Date Extracted 03/21/2002 <br /> [Client P Q Date Analyzed 03/21/2002 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 0203321-011 <br /> Client ID MW10/031802 <br /> Matrix W <br /> Compound Concentration* Rcpumng Limt Compound Concentration* Repomng UMLt <br /> Acetone ND 50 25 trans-1,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 10 5 0 Ethylene dibromide ND 1 0 50 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 1 0 5 0 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 10 50 Iodomethane ND 10 50 <br /> Bromoform ND 10 50 lsopropylbenzene ND 10 50 <br /> Brornomethane ND 1 0 5 0 p-Isopropyl toluene ND 10 5 0 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 1 0 5 0 <br /> sec-Butyl benzene ND 1 0 5 0 Methylene Chlonde` ND 1 0 5 0 <br /> tent-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND 1 0 5 0 Methyl isobutyl ketone ND 1 0 50 <br /> Carbon Tetrachloride ND 1 0 50 Methyl tent-Butyl Ether(MTBE) ND 1 0 5 0 <br /> Chlorobenzene ND 10 50 Naphthalene ND 5 0 25 <br /> Chloroethane ND<5 0 1 0 5 0 n-Propyl benzene ND 1 0 5 0 <br /> i <br /> 2-Chloroethyl Vinyl&th ND 1 0 5 0 Styrene ND 1 0 50 <br /> Chloroform ND to 50 1,1,1,2-Tetrachloroethane ND 1 0 50 <br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 1 0 5 0 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 10 5 0 <br /> 4-Chlomtoluene ND 1 0 5 0 Toluene ND 10 5 0 <br /> Dibromochloromethane ND 1 0 5 0 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 50 1,1,1-Tnchloroethane ND 10 50 <br /> 1,2-Dichlotobenzene ND 1 0 50 1,1,2-Trichloroethane ND 1 0 50 <br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 50 Tnchlomfluoromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Tnchloropropane ND 1 0 50 <br /> IJ-Dichloroethane ND 1 0 5 0 1,2,4-Tnmethylbenzene ND 1 0 5 0 <br /> 1,2-Dichloroethane ND 1 0 50 1,3,5-Tnmethylbenzene ND 1 0 5 0 <br /> I,1-Dichloroethene ND 1 0 50 Vinyl Acetate"I ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride " ND 10 5 0 <br /> tiaras-1,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 1 0 50 <br /> 1,2-Dichloropropane ND 1 0 5 0 Comments <br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%) <br /> 22-Dichloropropane ND 1 0 50 Dibromofluoromethane 96 <br /> I,l-Dichloropropene ND 10 50 Toluene-d8 93 <br /> cis-1 3-Dichloropropene ND 10 50 1 4-Bromofluorobenzene 85 <br /> `water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e)dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than--5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, i) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />