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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCC�BELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 - <br /> http://www.mccTnpbell.com E-mail: main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 12/15/00 <br /> 4005 North Wilson Way Date Received: 12/20/00 <br /> Stockton,CA 95205 Client Contact: Brian Millman Date Extracted: 12/22-12/26/00 <br /> Client P.O: Date Analyzed: 12122-12126/00 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 56443 <br /> Client ID MW 14/121500 <br /> Matrix W <br /> Reporting Limit * Reporting Limit <br />' Compound Concentration* �Compound Concentration <br /> W S W S <br /> Acetone ND<10 5.0 25 trans-1,3-Dichloropropene ND<10 1.0 5.0 <br /> Benzene 200 1.0 5.0 Ethylene dibromide ND<10 1.0 5.0 <br /> Bromobenzene ND<10 1.0 5.0 Ethyibenzene 63 1.0 5.0 <br /> Bromochloromethane ND<10 1.0 5.0 Ilexachlorobutadiene ND<10 5.0 25 <br /> Bromodichloromethanc ND<10 1.0 5.0 lodomethane ND<10 1.0 5.0 <br /> Bromoform ND<10 1.0 5.0 lsopropylbenzene ND<10 1.0 5.0 <br /> Bromomethane ND<10 1.0 5.0 p-Isopropyl toluene ND<10 1.0 5.0 <br /> n-Butyl benzene ND<10 1.0 5.0 Methyl butyl ketone mND<10 1.0 5.0 <br /> see-Butyl benzene ND<10 1.0 5.0 Methylene Chloride` ND<45 1.0 5.0 <br /> tert-Butyl benzene ND<10 1.0 5.0 Methyl ethyl ketone ND<10 2.0 10 <br /> Carbon Disulfide ND<10 1.0 5.0 Methyl isobutyl ketone ND<10 1.0 5A <br /> Carbon Tetrachloride ND<10 1.0 5.0 Methyl tert-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlorobenzenc ND<10 1.0 5.0 Naphthalene ND<10 5.0 5.0 <br /> Chloroethane ND<10 LO 5.0 n-Propyl benzene ND<10 1.0 5.0 <br /> 2-Chioroethyl Vinyl Eth ND<10 1.0 5.0 Styrene ND<]0 11.0 5.0 <br /> Chloroform ND<10 1.0 5.0 1,1,1,2-Tetrachloroethane ND<10 1.0 5.0 <br /> Chloromethane ND<10 1.0 5.0 1,1,2,2-Tetrachloroethane ND<10 1.0 5.0 <br /> 2-Chlorotoluene ND<10 1.0 5.0 Tetrachloroethene ND<20 1.0 5.0 <br />' 4-Chlorotoluene ND<10 1.0 5.0 Toluene 100 1.0 5.0 <br /> Dibromochloromethane ND<10 1.0 5.0 1,2,3-Trichlorobenzene ND<10 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND<10 2.0 10 1,2,4-Trichlorobenzene NIK10 5.0 25 <br /> Dibromomethane ND<10 1.0 5.0 1,1,1-Trichloroethane ND<10 1.0 5.0 <br />' 1,2-Dichlorobenzene ND<10 1.0 5.0 1,1,2-Trichloroethane ND<10 1.0 5.0 <br /> 1,3-Dichlorobenzene ND<10 1.0 5.0 Trichloroethene ND<10 1.0 5.0 <br /> 1,4-Dichlorobenzene ND<10 1.0 5.0 Trichlorofluoromethane ND<10 1.0 5.0 <br /> Dichlorodifluoromethane ND<10 1.0 5.0 1,2,3-Trichloropropane ND<10 1.0 5.0 <br />' l,l-Dichloroethane ND<10 1.0 5.0 1,2,4-Trimethylbenzene 140 1.0 5.0 <br /> 1,2-Dichloroethane 13 1.0 5.0 1,3,5-Trimethylbenzene 38 1.0 5.0 <br /> 1,1-Dichloroethene ND<10 1.0 5.0 Vinyl Acetate"I ND<10 5.0 25 <br /> cis-1,2-Dichloroethene ND<10 1.0 5.0 Vinyl Chloride " NiX10 1.0 1 5.0 <br />' trans-1,2-13ichloroethene ND<10 1.0 5.0 Xylenes,total 500 1.0 1 5.0 <br /> 1,2-Dichloropropane ND<10 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND<10 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<10 1.0 5.0 Dibromofluoromethane 105 <br />' 1,1-Dichloropropenc ND<10 1.0 5.0 Toluene-d8 101 <br /> cis-1,3-Dichloropropene ND<10 1.0 5.0 4-Bromofluorobenzene 103 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e)dichloromethane; (f) 2-butanone; (g)4-methyl-2- <br /> pentanone or isopropylacetonc; (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than-5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; l) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />' chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> 1 <br />