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110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax :925-798-1622 <br /> htto://www.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 01/18/00 <br /> 4005 North Wilson Way Date Received: 01/19/00 <br /> Stockton,CA 95205 Client Contact: Kevin McKibben Date Extracted: 01/21-01/24/00 <br /> Client P.O: Date Analyzed: 01121-01124100 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 29317 <br /> Client ID MW-811-18-00 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone c6 ND<30 trans-1,3-Dichloropropene ND<2.5 <br /> Benzene ND<2.5 Ethylene dibromide ND<2.5 <br /> Bromobenzene ND<2.5 Ethylbenzene 53 <br /> Bromochloromethane ND<2.5 Hexachlorobutadiene ND<2.5 <br /> Bromodichloromethane ND<2.5 lodomethane ND<2.5 <br /> Bromoform NIX2.5 lsopropylbenzene 13 <br /> Bromomethane ND<2.5 p4sopropyl toluene ND<2.5 <br /> n-Butyl benzene 4.9 Methyl butyl ketone ND<2.5 <br /> sec-Butyl benzene 4.9 Methylene Chloride`' ND<10 <br /> tert-Butyl benzene 4.0 Methyl ethyl ketone ' ND<2.5 <br /> Carbon Disulfide ND<2.5 Methyl isobutyl ketone 4e1 ND<2.5 <br /> Carbon Tetrachloride ND<2.5 Methyl tert-Butyi Ether(MTBE) --- <br /> Chlorobenzene ND<2.5 Naphthalene ND<2.5 <br /> Chloroethane ND<2.5 n-Propyl benzene 22 <br /> 2-Chloroethyl Vinyl Ether" ND<2.5 Styrene` ND<2.5 <br /> Chloroform ND<2.5 1,1,1,2-Tetrachloroethane 1.'1X2.5 <br /> Chloromethane N D<2.5 1,1,2,2-Tetrachloroethane ND<2.5 <br /> 2-Chlorotoluene ND<2.5 Tetrachloroethene 3.0 <br /> 4-Chlorotoluene ND<2.5 Toluene'"' 4.2 <br /> Dibromochloromethane ND<2.5 1,2,3-Trichlorobenzene ND<2.5 <br /> 1,2-Dibromo-3-chloropmpane ND<2.5 1,2,4-Trichlorobenzene ND<2.5 <br /> Dibromomethan e ND<2.5 1,1,1-Trichloroethane ND<2.5 <br /> 1,2-Dichlorobenzene ND<2.5 1,1,2-Trichloroethane ND<2.5 <br /> 1,3-Dichlorobenzene ND<2.5 Trichloroethene ND<2.5 <br /> 1,4-Dichlorobenzene ND<2.5 Trichlorofluoromethane ND<2.5 <br /> Dichlorodifluoromethane ND<2.5 1,2,3-Trichloropropane ND<2.5 <br /> 1,1-Dichloroethane ND<2.5 1,2,4-Trimethylbenzene 91 <br /> 1,2-Dichloroethane 5.2 1,3,5-Trimethylbenzene 27 <br /> l,l-Dichloroethene ND<2.5 Vinyl Acetate"" ND<2.5 <br /> cis-1,2-Dichloroethene ND<2.5 Vinyl Chloride'°' ND<2.5 <br /> trans-1,2-Dichloroethene ND<2.5 Xylenes,total ° 76 <br /> 1,2-Dichloropropane ND<2.5 Comments: <br /> 1,3-Dichloropropane ND<2.5 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<2.5 Dibromofluorotnethane 99 <br /> 1,1-Dichloropropene ND<2.5 Toluene-d8 92 <br /> cis-1,3-Dichloropropene ND<2.5 4-Bromofluorobenzene 85 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 uglkg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e)dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i) liquid sample that contains greater than--5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />