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i110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 <br /> http:l/www.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnviromnental Client Project ID:Geweke Date Sampled: 09/30/99 <br /> 4005 North Wilson Way Date Received: 10/02/99 <br /> Stockton,CA 95205 Client Contact: Kevin McKibben Date Extracted: 10/07-10/12/99 <br /> Client P.O: Date Analyzed: 10/07-10/12/99 <br /> I Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 22673 <br /> Client ID MW6 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetonem ND<5 trans-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide ND <br />'f Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND lodomethane ND <br /> I Bromoform ND Isopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone` ND <br /> sec-Butyl benzene ND Methylene Chloride"' ND <br /> I tent-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide ND Methyl isobutyl ketones ND <br /> Carbon Tetrachloride ND Methyl tent-Butyl Ether(MTBE) <br /> Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether") ND Styrene ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene(.) ND <br /> Dibromochloromethane ND 1,2,3-TriChlorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> _.l,I-Dichloroethane ND 1,2,4-Trimethylbenzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Trimethylbenzene ND <br /> I,I-Dichloroethene ND Vinyl Acetate ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride ND <br /> trans-1,2-Dichloroethene ND Xylenes,total wl ND <br /> 1,2-Dichloropropane ND Comments: <br /> I 1,3-Dichloropropane ND Surrogate Recoveries <br /> 2,2-Dichloropropane ND Dibromofluoromethane 124 <br /> 1,1-Dichloropropene ND Toluene-d8 102 <br /> cis-1,3-Dichloropropene ND 4-Bromotluorobenzene 97 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in us/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples I ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanonc; (e) dichloromethane; (t) 2-butanone; (g) 4-methyl-2 <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroetbene;(o)dimethylbenzenes. on <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director. <br /> I <br />