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. 110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax : 925-798-1622 <br /> bqp://www.mccampbell.com E-mail:main@mceampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 09/30/99 <br /> 4005 North Wilson Way Date Received: 10/02/99 <br /> IStockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 10/07-10/12/99 <br /> Client P.O: Date Analyzed: 10/07-10/12199 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 22675 <br /> Client ID MW11 <br /> Matrix W <br /> Compound Concentration* Compound Concentration' <br /> Acetone ND<5 trans-l,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene NO <br /> Bromochloromethane NO Hexachlorobutadiene ND <br /> Bromodichloromethane NO lodomethane NO <br /> Bromoform NO lsopropylbenzene ND <br /> Bromomethane ND p4sopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone NO <br /> sec-Butyl benzene 3.1 Methylene Chloride"' ND <br /> ten-Butyl benzene <br /> NO Methyl ethyl ketone NO <br /> Carbon Disulfide NO Methyl isobutyl ketone ND <br /> Carbon Tetrachloride NO Methyl ter(-Butyl Ether(MTBE) --- <br /> Chlorobenzene NO Naphthalene ND <br /> Chloroethane NO n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ethe NO Styrene NO <br /> Chloroform NO 1,1,1,2-Tetrachloroethane NO <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane NO <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoiuene ND Toluene(MiND <br /> Dibromochloromethane NO 1,2,3-Trichlorobenzene ND <br /> E 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorobenzene NO <br /> Dibromomethane NO 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane NO <br /> 1,3-Dichlorobenzene NO Trichloroethene NO <br /> 1,4-Dichlorobenzene NO Trichlorofluoromethane NO <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> l,l-Dichloroethane ND 1,2,4-Trimethylbenzene NO <br /> 1,2-Dichloroethane ND 1,3,5-Trimethylbenzene ND <br /> l,l-Dichloroethene ND Vinyl Acetate NO <br /> cis-1,2-Dichloroethene ND Vinyl Chloride ND <br /> trans-l,2-Dichloroethene NO Xylenes,total 1.4 <br /> 1,2-Dichloropropane NO Comments: <br /> 1,3-Dichloropropane ND Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 120 <br /> 1,1-Dichloropropene NO Toluene-d8 100 <br /> cis-1,3-Dichloropropene NO 4-Bromofluorobenzene 93 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> E <br /> NO means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g)4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (]}methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> E chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br /> E .. . <br />